2-cyclohexyl-2-methylpropane-1,3-diyl dicarbamate

Base Information

• Chemical Name: 2-cyclohexyl-2-methylpropane-1,3-diyl dicarbamate
• CAS No.: 1146-18-5
• Molecular Formula: C₁₂H₂₂N₂O₄
• Molecular Weight: 258.318
• Mol file: 1146-18-5.mol

Synonyms:1,3-Propanediol,2-cyclohexyl-2-methyl-, dicarbamate (8CI); Carbamic acid, 2-cyclohexyl-2-methyltrimethyleneester (7CI)

Chemical Property of 2-cyclohexyl-2-methylpropane-1,3-diyl dicarbamate

Chemical Property:

• Vapor Pressure: 1.41E-09mmHg at 25°C
• Boiling Point: 485.4°Cat760mmHg
• Flash Point: 241.4°C
• Density: 1.173g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-cyclohexyl-2-methylpropane-1,3-diyl dicarbamate

There total 4 articles about 2-cyclohexyl-2-methylpropane-1,3-diyl dicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-cyclohexylpropanal) (2109-22-0) → 1-Carbamoyloxy-2-carbamoyloxymethyl-2-cyclohexyl-propan (1146-18-5)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. Na₂CO₃

2: Al(OiPr)3 / xylene / Heating

With aluminum isopropoxide; sodium carbonate; In xylene;

Reference yield:

2-Cyclohexyl-1-methoxy-propan-2-ol (2109-96-8) → 1-Carbamoyloxy-2-carbamoyloxymethyl-2-cyclohexyl-propan (1146-18-5)

Guidance literature:

Multi-step reaction with 3 steps

1: ion-exchange resin + form>

2: aq. Na₂CO₃

3: Al(OiPr)3 / xylene / Heating

With ion-exchange resin + form>; aluminum isopropoxide; sodium carbonate; In xylene;

Reference yield:

2-Methyl-2-cyclohexyl-propandiol-(1,3) (2037-62-9) + urethane (51-79-6) → 1-Carbamoyloxy-2-carbamoyloxymethyl-2-cyclohexyl-propan (1146-18-5)

Guidance literature:

With aluminum isopropoxide; In xylene; Heating;

upstream raw materials:

2-Methyl-2-cyclohexyl-propandiol-(1,3)

urethane

(2-cyclohexylpropanal)

2-Cyclohexyl-1-methoxy-propan-2-ol