2-(2,4-Dinitrophenoxy)ethanol

Base Information

• Chemical Name: 2-(2,4-Dinitrophenoxy)ethanol
• CAS No.: 2831-60-9
• Molecular Formula: C8H8N2O6
• Molecular Weight: 228.161
• Hs Code.: 2909499000
• European Community (EC) Number: 220-597-3
• NSC Number: 28669
• DSSTox Substance ID: DTXSID8062656
• Nikkaji Number: J306.764E
• Wikidata: Q81990173
• Mol file: 2831-60-9.mol

Synonyms:2-(2,4-Dinitrophenoxy)ethanol;2831-60-9;Ethanol, 2-(2,4-dinitrophenoxy)-;2,4-Dinitrophenoxyethanol;1-(2-Hydroxyethoxy)-2,4-dinitrobenzene;Ethanol,2-(2,4-dinitrophenoxy)-;2-(2,4-dinitrophenoxy)ethan-1-ol;beta-Hydroxyethyl 2,4-dinitrophenyl ether;EINECS 220-597-3;MFCD00052808;NSC 28669;.beta.-Hydroxyethyl 2,4-dinitrophenyl ether;Maybridge1_002900;Ethanol,4-dinitrophenoxy)-;DivK1c_001652;SCHEMBL4101417;DTXSID8062656;HMS549L18;2-(2,4-dinitrophenoxy) ethanol;2-(2',4'-dinitrophenoxy)ethanol;2-(2,4 -dinitrophenoxy) ethanol;NSC28669;2-(2',4'-dinitrophenoxy)-ethanol;2-(2,4-dinitrophenoxy)-1-ethanol;CCG-53396;NSC-28669;2-(2',4'-dinitro-phenoxy)-ethanol;AKOS000505948;CDS1_000612;CD 08003;SY122175;CS-0320555;H10639;SR-01000642563-1

Chemical Property of 2-(2,4-Dinitrophenoxy)ethanol

Chemical Property:

• Vapor Pressure: 1.65E-08mmHg at 25°C
• Refractive Index: 1.607
• Boiling Point: 439.7 °C at 760 mmHg
• Flash Point: 219.7 °C
• PSA: 121.10000
• Density: 1.509 g/cm³
• LogP: 1.92050
• XLogP3: 1.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 3
• Exact Mass: 228.03823598
• Heavy Atom Count: 16
• Complexity: 260

Purity/Quality:

98%,99%, ^*data from raw suppliers

2-(2,4-Dinitrophenoxy)ethanol ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C=C1[N+](=O)[O-])[N+](=O)[O-])OCCO

Technology Process of 2-(2,4-Dinitrophenoxy)ethanol

There total 10 articles about 2-(2,4-Dinitrophenoxy)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

ethylene glycol (107-21-1) + 1-chloro-2,4-dinitro-benzene (97-00-7) → 2-(2,4-dinitrophenoxy)ethanol (2831-60-9)

Guidance literature:

ethylene glycol; 1-chloro-2,4-dinitro-benzene; at 78 ℃; for 0.5h;

With sodium hydroxide; at 85 - 95 ℃; for 2.66667h;

In water; at 90 ℃; for 1.66667h; Concentration;

Reference yield: 95.6%

oxirane (75-21-8,99932-75-9) + 1-chloro-2,4-dinitro-benzene (97-00-7) → 2-(2,4-dinitrophenoxy)ethanol (2831-60-9)

Guidance literature:

1-chloro-2,4-dinitro-benzene; With water; potassium hydroxide; at 90 ℃; for 1h;

oxirane; for 5h; Reagent/catalyst;

Reference yield:

(2,4-dinitro-phenyl)-(4-nitro-phenyl)-ether (2363-36-2) + ethylene glycol (107-21-1) → 4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + 2-(2,4-dinitrophenoxy)ethanol (2831-60-9)

Guidance literature:

Kinetics;

DOI:10.1021/ja01177a077

upstream raw materials:

2,4-dinitroanisole

ethylene glycol

2,4-dinitrophenyl phenyl ether

1-chloro-2,4-dinitro-benzene

Downstream raw materials:

1-(2,4-dinitro-phenoxy)-2-nitryloxy-ethane

2,4-diamino-1-(β-hydroxyethyloxy)benzene

2-(2-amino-4-nitro-phenoxy)-ethanol

Allyl 2,4-dinitrophenyl ether