2,3,8-trimethoxy-6-methyl-6,11-dihydro-2H-indeno[1,2-c]isoquinolin-9-ol

Base Information

Chemical Name:2,3,8-trimethoxy-6-methyl-6,11-dihydro-2H-indeno[1,2-c]isoquinolin-9-ol
CAS No.:96705-56-5
Molecular Formula:C20H20ClNO4
Molecular Weight:373.836
Hs Code.:

Synonyms:11H-Indeno[1,2-c]isoquinolinium, 9-hydroxy-2,3, 8-trimethoxy-6-methyl-, chloride;2,3,8-Trimethoxy-6-methyl-11H-6.lambda.~5~-indeno[1,2-c]isoquinolin-9-ol;Indenoisoquinoline analogue of fagaronine chloride;{11H-Indeno[1,2-c]isoquinolinium,} 9-hydroxy-2,3, 8-trimethoxy-6-methyl-, chloride;9-Hydroxy-6-methyl-2,3,8-trimethoxy-11H-indeno(1,2-c)isoquinolinium chloride;

Suppliers and Price of 2,3,8-trimethoxy-6-methyl-6,11-dihydro-2H-indeno[1,2-c]isoquinolin-9-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 6 raw suppliers

Chemical Property of 2,3,8-trimethoxy-6-methyl-6,11-dihydro-2H-indeno[1,2-c]isoquinolin-9-ol

Chemical Property:

Vapor Pressure:2.6E-18mmHg at 25°C
Refractive Index:1.657
Boiling Point:°Cat760mmHg
Flash Point:°C
Density:g/cm³

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,3,8-trimethoxy-6-methyl-6,11-dihydro-2H-indeno[1,2-c]isoquinolin-9-ol

There total 1 articles about 2,3,8-trimethoxy-6-methyl-6,11-dihydro-2H-indeno[1,2-c]isoquinolin-9-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5653-42-9
3,4-dimethoxyhomophthalic anhydride

: 96705-56-5
2,3,8-trimethoxy-6-methyl-9-hydroxy-11H-indeno<1,2-c>isoquinolinium chloride

Guidance literature:: Multi-step reaction with 5 steps

1: 35 percent / CHCl₃ / 0.5 h / Ambient temperature

2: 42 percent / P₂O₅ / 21 h / 60 - 70 °C

3: 80 percent / BH₃ / tetrahydrofuran / 4 h / Heating

4: 100 percent / KOH / H₂O; ethanol / 1 h / Heating

5: 55 percent / 5percent Pd/C / acetic acid / 24 h / Heating

With potassium hydroxide; borane; phosphorus pentoxide; palladium on activated charcoal; In tetrahydrofuran; ethanol; chloroform; water; acetic acid;
DOI:10.1021/jm00146a010