2-Methoxynaphthalene-1-carbonyl chloride

Base Information

Chemical Name:2-Methoxynaphthalene-1-carbonyl chloride
CAS No.:51439-58-8
Molecular Formula:C12H9 Cl O2
Molecular Weight:220.655
Hs Code.:2918990090
European Community (EC) Number:257-205-5
DSSTox Substance ID:DTXSID50199413
Nikkaji Number:J261.724B
Wikidata:Q83072332
Mol file:51439-58-8.mol

Synonyms:2-Methoxynaphthalene-1-carbonyl chloride;51439-58-8;2-methoxy-1-naphthoyl chloride;EINECS 257-205-5;2-methoxy-naphthalene-1-carbonyl chloride;SCHEMBL3997233;DTXSID50199413;SXPBNKRSGVLWJQ-UHFFFAOYSA-N;AM20040603;2-Methoxy-1-naphthalenecarboxylic acid chloride

Suppliers and Price of 2-Methoxynaphthalene-1-carbonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
2-Methoxynaphthalene-1-carbonylchloride 97%
1g
$ 638.00

Atlantic Research Chemicals
2-Methoxynaphthalene-1-carbonylchloride 95%
1gm:
$ 265.09

Alichem
2-Methoxynaphthalene-1-carbonylchloride
500mg
$ 1048.60

Total 7 raw suppliers

Chemical Property of 2-Methoxynaphthalene-1-carbonyl chloride

Chemical Property:

Vapor Pressure:1.6E-05mmHg at 25°C
Boiling Point:365.2°Cat760mmHg
Flash Point:134.7°C
PSA：26.30000
Density:1.268g/cm³
LogP:3.22740
XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:220.0291072
Heavy Atom Count:15
Complexity:242

Purity/Quality:

99%, ^*data from raw suppliers

2-Methoxynaphthalene-1-carbonylchloride 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C2=CC=CC=C2C=C1)C(=O)Cl

Technology Process of 2-Methoxynaphthalene-1-carbonyl chloride

There total 5 articles about 2-Methoxynaphthalene-1-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 947-62-6
2-methoxy-1-naphthoic acid

: 51439-58-8
2-methoxy-1-naphthoic acid chloride

Guidance literature:: With thionyl chloride;
DOI:10.1246/bcsj.76.575

Reference yield:

: 883-21-6
1-methoxy-2-naphthoic acid

: 51439-58-8
2-methoxy-1-naphthoic acid chloride

Guidance literature:: With thionyl chloride; for 2h; Heating / reflux;

Reference yield:

: 3401-47-6
1-bromo-2-methoxynaphthalene

: 51439-58-8
2-methoxy-1-naphthoic acid chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) t-BuLi / 1.) THF, pentane, -78 deg C, 1 h, 2.) THF, pentane, from -78 deg C to RT, 1 h

2: oxalyl chloride / CH₂Cl₂ / 5 h

With oxalyl dichloride; tert.-butyl lithium; In dichloromethane;
DOI:10.1021/ja00029a032