Tungsten, tetracarbonyl(piperidine)(triphenylphosphine)-

Base Information

Chemical Name:Tungsten, tetracarbonyl(piperidine)(triphenylphosphine)-
CAS No.:67010-37-1
Molecular Formula:C27H26NO4PW
Molecular Weight:643.332
Hs Code.:

Synonyms:

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Chemical Property of Tungsten, tetracarbonyl(piperidine)(triphenylphosphine)-

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Technology Process of Tungsten, tetracarbonyl(piperidine)(triphenylphosphine)-

There total 2 articles about Tungsten, tetracarbonyl(piperidine)(triphenylphosphine)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 14515-95-8,56083-13-7
cis-(tungsten tetracarbonyl bipiperidine)

: 603-35-0
triphenylphosphine

: 38496-27-4,67010-37-1
cis-(piperidine)(triphenylphosphine)W(CO)4

Guidance literature:: In dichloromethane; for 0.166667h; Inert atmosphere; Schlenk technique; Reflux;
DOI:10.1007/s10870-018-0743-1

Reference yield:

: 110-89-4
piperidine

: 118818-76-1
{(C₆H₅Cl)(P(C₆H₅)3)W(CO)4}

: 38496-27-4,67010-37-1
cis-(piperidine)(triphenylphosphine)W(CO)4

Guidance literature:: In chlorobenzene; High Pressure; photolysis of substrate in PhCl carried out with Nd:YAG laser (355 nm) at 5 to 150 MPa and 24.5°C; not isolated; monitored at 455 nm; Kinetics;
DOI:10.1039/c39870001839

Reference yield: 70.0%

: 67010-37-1
W(CO)4P(C₆H₅)3(NH(CH₂)5)

: 21050-13-5
bis(triphenylphosphine)iminium chloride

: 82963-30-2
[(triphenylphosphine)2N][cis-[WH(CO)4(triphenylphosphine)]]

Guidance literature:: With sodium naphthalenide; MeOH; In tetrahydrofuran; Na naphthalenide was added to soln. of W complex at -78°C (Ar, N2); at the same temp. PPNCl in MeOH was added; warming to room temp.; evapn., extn. with THF; filtration through Celite; pptn. with hexane; sepn., drying in vac.;