3-Oxazolidinecarboxylic acid, 4-[4-[[[(1S)-1-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-methoxy-2- oxoethyl]amino]carbonyl]-5-methyl-2-oxazolyl]-2,2,5-trimethyl-, phenylmethyl ester, (4S,5R)-

Base Information

Chemical Name:3-Oxazolidinecarboxylic acid, 4-[4-[[[(1S)-1-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-methoxy-2- oxoethyl]amino]carbonyl]-5-methyl-2-oxazolyl]-2,2,5-trimethyl-, phenylmethyl ester, (4S,5R)-
CAS No.:670233-35-9
Molecular Formula:C₃₉H₄₇N₃O₈Si
Molecular Weight:713.903
Hs Code.:

3-Oxazolidinecarboxylic acid,
4-[4-[[[(1S)-1-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-methoxy-2-
oxoethyl]amino]carbonyl]-5-methyl-2-oxazolyl]-2,2,5-trimethyl-,
phenylmethyl ester, (4S,5R)-

Synonyms:

Suppliers and Price of 3-Oxazolidinecarboxylic acid, 4-[4-[[[(1S)-1-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-methoxy-2- oxoethyl]amino]carbonyl]-5-methyl-2-oxazolyl]-2,2,5-trimethyl-, phenylmethyl ester, (4S,5R)-

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Chemical Property of 3-Oxazolidinecarboxylic acid, 4-[4-[[[(1S)-1-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-methoxy-2- oxoethyl]amino]carbonyl]-5-methyl-2-oxazolyl]-2,2,5-trimethyl-, phenylmethyl ester, (4S,5R)-

Chemical Property:

Purity/Quality:

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Technology Process of 3-Oxazolidinecarboxylic acid, 4-[4-[[[(1S)-1-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-methoxy-2- oxoethyl]amino]carbonyl]-5-methyl-2-oxazolyl]-2,2,5-trimethyl-, phenylmethyl ester, (4S,5R)-

There total 6 articles about 3-Oxazolidinecarboxylic acid, 4-[4-[[[(1S)-1-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-methoxy-2- oxoethyl]amino]carbonyl]-5-methyl-2-oxazolyl]-2,2,5-trimethyl-, phenylmethyl ester, (4S,5R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 160821-18-1
(4S,5R)-3-((benzyloxy)carbonyl)-2,2,5-trimethyloxazolidine-4-carboxylic acid

: 670233-35-9
(4'S,5'R)-4-[(S)-2-(tert-Butyl-diphenyl-silanyloxy)-1-methoxycarbonyl-ethylcarbamoyl]-5,2',2',5'-tetramethyl-4',5'-dihydro-[2,4']bioxazolyl-3'-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 6 steps

1.1: 92 percent / DCC; HOBt / dimethylformamide

2.1: MsCl; NEt₃ / CHCl₃

2.2: DBU / CHCl₃

3.1: NBS / tetrahydrofuran

3.2: Et₃N / tetrahydrofuran

4.1: Cs₂CO₃ / dioxane

5.1: 100 percent / LiOH / dioxane; H₂O

6.1: DPPA; Et₃N / dimethylformamide

With lithium hydroxide; N-Bromosuccinimide; diphenyl-phosphinic acid; benzotriazol-1-ol; caesium carbonate; methanesulfonyl chloride; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1246/cl.2004.72

Reference yield:

: (4S,5R)-4-((Z)-1-Methoxycarbonyl-propenylcarbamoyl)-2,2,5-trimethyl-oxazolidine-3-carboxylic acid benzyl ester

: 670233-35-9
(4'S,5'R)-4-[(S)-2-(tert-Butyl-diphenyl-silanyloxy)-1-methoxycarbonyl-ethylcarbamoyl]-5,2',2',5'-tetramethyl-4',5'-dihydro-[2,4']bioxazolyl-3'-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: NBS / tetrahydrofuran

1.2: Et₃N / tetrahydrofuran

2.1: Cs₂CO₃ / dioxane

3.1: 100 percent / LiOH / dioxane; H₂O

4.1: DPPA; Et₃N / dimethylformamide

With lithium hydroxide; N-Bromosuccinimide; diphenyl-phosphinic acid; caesium carbonate; triethylamine; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1246/cl.2004.72

Reference yield:

: 670233-33-7
(4'S,5'R)-5,2',2',5'-Tetramethyl-4',5'-dihydro-[2,4']bioxazolyl-4,3'-dicarboxylic acid 3'-benzyl ester 4-methyl ester

: 670233-35-9
(4'S,5'R)-4-[(S)-2-(tert-Butyl-diphenyl-silanyloxy)-1-methoxycarbonyl-ethylcarbamoyl]-5,2',2',5'-tetramethyl-4',5'-dihydro-[2,4']bioxazolyl-3'-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / LiOH / dioxane; H₂O

2: DPPA; Et₃N / dimethylformamide

With lithium hydroxide; diphenyl-phosphinic acid; triethylamine; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1246/cl.2004.72