Thieno[2,3-b]pyridine-5-carboxamide, N-[(4-chlorophenyl)methyl]-2-[[[2-(3-cyanophenyl)-2-hydroxyethyl]methyl amino]methyl]-4,7-dihydro-7-methyl-4-oxo-

Base Information

Chemical Name:Thieno[2,3-b]pyridine-5-carboxamide, N-[(4-chlorophenyl)methyl]-2-[[[2-(3-cyanophenyl)-2-hydroxyethyl]methyl amino]methyl]-4,7-dihydro-7-methyl-4-oxo-
CAS No.:672326-40-8
Molecular Formula:C27H25ClN4O3S
Molecular Weight:521.039
Hs Code.:

Thieno[2,3-b]pyridine-5-carboxamide,
N-[(4-chlorophenyl)methyl]-2-[[[2-(3-cyanophenyl)-2-hydroxyethyl]methyl
amino]methyl]-4,7-dihydro-7-methyl-4-oxo-

Synonyms:

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Chemical Property of Thieno[2,3-b]pyridine-5-carboxamide, N-[(4-chlorophenyl)methyl]-2-[[[2-(3-cyanophenyl)-2-hydroxyethyl]methyl amino]methyl]-4,7-dihydro-7-methyl-4-oxo-

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Technology Process of Thieno[2,3-b]pyridine-5-carboxamide, N-[(4-chlorophenyl)methyl]-2-[[[2-(3-cyanophenyl)-2-hydroxyethyl]methyl amino]methyl]-4,7-dihydro-7-methyl-4-oxo-

There total 4 articles about Thieno[2,3-b]pyridine-5-carboxamide, N-[(4-chlorophenyl)methyl]-2-[[[2-(3-cyanophenyl)-2-hydroxyethyl]methyl amino]methyl]-4,7-dihydro-7-methyl-4-oxo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 672326-01-1
N-(4-chlorobenzyl)-2-(chloromethyl)-7-methyl-4-oxo-4,7-dihydrothieno[2,3-b]-pyridine-5-carboxamide

: rac-3-(1-hydroxy-2-(methylamino)ethyl)benzonitrile

: 672326-40-8
C₂₇H₂₅N₄SO₃Cl

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2007.03.102

Reference yield:

: 292144-09-3
N-(4-chlorobenzyl)-2-(hydroxymethyl)-7-methyl-4-oxo-4,7-dihydrothieno[2,3-b]-pyridine-5-carboxamide

: 672326-40-8
C₂₇H₂₅N₄SO₃Cl

Guidance literature:: Multi-step reaction with 2 steps

1: methanesulfonyl chloride; 2,4,6-collidine; DMAP / dimethylformamide

2: i-Pr₂EtN / dimethylformamide

With 2,4,6-trimethyl-pyridine; dmap; methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2007.03.102

Reference yield:

: 292144-10-6
PNU-243672

: 672326-40-8
C₂₇H₂₅N₄SO₃Cl

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / ethyl chloroformate / CHCl₃ / Heating

2: i-Pr₂EtN / dimethylformamide

With chloroformic acid ethyl ester; N-ethyl-N,N-diisopropylamine; In chloroform; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2007.03.102