2-Chloro-5-methoxybenzene-1,4-diol

Base Information

• Chemical Name: 2-Chloro-5-methoxybenzene-1,4-diol
• CAS No.: 67289-06-9
• Molecular Formula: C₇H₇ClO₃
• Molecular Weight: 174.584
• DSSTox Substance ID: DTXSID80497914
• Nikkaji Number: J801.989D
• Wikidata: Q82347685

Synonyms:2-Chloro-5-methoxybenzene-1,4-diol;67289-06-9;SCHEMBL69147;DTXSID80497914

Chemical Property of 2-Chloro-5-methoxybenzene-1,4-diol

Chemical Property:

• XLogP3: 2.3
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 174.0083718
• Heavy Atom Count: 11
• Complexity: 131

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=C(C=C(C(=C1)O)Cl)O

Technology Process of 2-Chloro-5-methoxybenzene-1,4-diol

There total 2 articles about 2-Chloro-5-methoxybenzene-1,4-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-chlorovaniline (18268-76-3) → 2-chloro-5-methoxy-hydroquinone (67289-06-9)

Guidance literature:

With sodium hydroxide; dihydrogen peroxide;

Reference yield:

→ 2-chloro-5-methoxy-hydroquinone (67289-06-9)

Guidance literature:

2-Methoxy-1,4-chinon 1. (CH3)3SiCl 2. CH3CN 3. W.;

DOI:10.1021/jo00409a039

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + 2-chloro-5-methoxy-hydroquinone (67289-06-9) → 1-chloro-2,4,5-trimethoxybenzene (20129-10-6)

Guidance literature:

With diethyl ether;

upstream raw materials:

6-chlorovaniline

Downstream raw materials:

1-chloro-2,4,5-trimethoxybenzene

5-chloro-2-methoxy-p-hydroquinone diacetate

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