3-Allyl-4,5-dimethoxy-benzaldehyde

Base Information

• Chemical Name: 3-Allyl-4,5-dimethoxy-benzaldehyde
• CAS No.: 67483-49-2
• Molecular Formula: C12H14O3
• Molecular Weight: 206.241
• DSSTox Substance ID: DTXSID60389767
• Nikkaji Number: J2.243.751H
• Wikidata: Q82185897
• Mol file: 67483-49-2.mol

Synonyms:3-Allyl-4,5-dimethoxy-benzaldehyde;67483-49-2;3-ALLYL-4,5-DIMETHOXYBENZALDEHYDE;3,4-dimethoxy-5-prop-2-enylbenzaldehyde;3,4-dimethoxy-5-(prop-2-en-1-yl)benzaldehyde;SCHEMBL9164276;DTXSID60389767;FBLUJEZNJVZMKK-UHFFFAOYSA-N;MFCD02629560;AKOS000290651;FT-0722289

Chemical Property of 3-Allyl-4,5-dimethoxy-benzaldehyde

Chemical Property:

• Vapor Pressure: 0.000451mmHg at 25°C
• Boiling Point: 315oC at 760 mmHg
• Flash Point: 135.3oC
• PSA: 35.53000
• Density: 1.065g/cm3
• LogP: 2.24480
• XLogP3: 2.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 5
• Exact Mass: 206.094294304
• Heavy Atom Count: 15
• Complexity: 215

Purity/Quality:

98%min ^*data from raw suppliers

3-Allyl-4,5-dimethoxybenzaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC(=CC(=C1OC)CC=C)C=O

Technology Process of 3-Allyl-4,5-dimethoxy-benzaldehyde

There total 9 articles about 3-Allyl-4,5-dimethoxy-benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

3-allyl-4-hydroxy-5-methoxybenzaldehyde (20240-58-8) + methyl iodide (74-88-4) → 3,4-dimethoxy-5-(prop-2-enyl)benzaldehyde (67483-49-2)

Guidance literature:

With potassium carbonate; In ethanol; for 4h; Reflux;

DOI:10.1016/j.tet.2008.08.005

Reference yield: 92.0%

→ 3,4-dimethoxy-5-(prop-2-enyl)benzaldehyde (67483-49-2)

Guidance literature:

Reference yield: 80.0%

3-allyl-4-hydroxy-5-methoxybenzaldehyde (20240-58-8) + dimethyl sulfate (77-78-1) → 3,4-dimethoxy-5-(prop-2-enyl)benzaldehyde (67483-49-2)

Guidance literature:

3-allyl-4-hydroxy-5-methoxybenzaldehyde; With benzyltrimethylammonium chloride; sodium hydroxide; In water;

dimethyl sulfate; In water; at 0 - 20 ℃;

DOI:10.1016/j.ejmech.2018.06.025

upstream raw materials:

3-allyl-4-hydroxy-5-methoxybenzaldehyde

1-allyl-2,3-dimethoxy-benzene

N-methyl-N-phenylformamide

methyl iodide

Downstream raw materials:

4,5-dimethoxy-isophthalic acid

(5-dimethoxymethyl)-1,2-dimethoxy-3-(prop-2-enyl)benzene

di-(2-ethylhexyl) 3-allyl-4,5-dimethoxybenzalmalonate

E-1-allyl-2,3-dimethoxy-5-(20-nitrovinyl)benzene