1,3-Dioxane, 2-(3-bromo-4-methylphenyl)-5,5-dimethyl-

Base Information

Chemical Name:1,3-Dioxane, 2-(3-bromo-4-methylphenyl)-5,5-dimethyl-
CAS No.:675824-20-1
Molecular Formula:C13H17BrO2
Molecular Weight:285.181
Hs Code.:
DSSTox Substance ID:DTXSID80477837
Wikidata:Q82310817

Synonyms:675824-20-1;1,3-Dioxane, 2-(3-bromo-4-methylphenyl)-5,5-dimethyl-;DTXSID80477837

Suppliers and Price of 1,3-Dioxane, 2-(3-bromo-4-methylphenyl)-5,5-dimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1,3-Dioxane, 2-(3-bromo-4-methylphenyl)-5,5-dimethyl-

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:284.04119
Heavy Atom Count:16
Complexity:232

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C=C(C=C1)C2OCC(CO2)(C)C)Br

Technology Process of 1,3-Dioxane, 2-(3-bromo-4-methylphenyl)-5,5-dimethyl-

There total 2 articles about 1,3-Dioxane, 2-(3-bromo-4-methylphenyl)-5,5-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 36276-24-1
3-bromo-4-methyl-benzaldehyde

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 675824-20-1
1-bromo-2-methyl-5-(4,4-dimethyl-2,6-dioxan-1-yl)benzene

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 18h; Heating;
DOI:10.1039/b312898a

Reference yield:

: 104-87-0
4-methyl-benzaldehyde

: 675824-20-1
1-bromo-2-methyl-5-(4,4-dimethyl-2,6-dioxan-1-yl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: AlCl₃ / CH₂Cl₂ / 0.5 h / 40 °C

1.2: 89 percent / bromine / CH₂Cl₂ / 0.5 h / 30 - 40 °C

2.1: 96 percent / p-toluenesulfonic acid / benzene / 18 h / Heating

With aluminium trichloride; toluene-4-sulfonic acid; In dichloromethane; benzene;
DOI:10.1039/b312898a