Technology Process of Grevillol
There total 19 articles about Grevillol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen bromide; acetic acid;
for 3h;
Heating;
DOI:10.1021/jo9610624
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) Mg, I2
2: p-TsOH / benzene
3: 89 percent / H2 / 10percent Pd/C
4: BBr3 / CH2Cl2
With
hydrogen; iodine; boron tribromide; toluene-4-sulfonic acid; magnesium;
palladium on activated charcoal;
In
dichloromethane; benzene;
DOI:10.1021/ja00156a004
- Guidance literature:
-
Multi-step reaction with 2 steps
1: H2 / 10percent Pd/C / ethyl acetate / 12 h / 25 °C
2: BBr3 / CH2Cl2 / 12 h / 0 - 25 °C
With
hydrogen; boron tribromide;
palladium on activated charcoal;
In
dichloromethane; ethyl acetate;
DOI:10.1021/ja00219a046
