1-(Bromomethyl)cyclohexan-1-ol

Base Information

• Chemical Name: 1-(Bromomethyl)cyclohexan-1-ol
• CAS No.: 17299-10-4
• Molecular Formula: C7H13 Br O
• Molecular Weight: 193.084
• European Community (EC) Number: 828-295-9
• NSC Number: 175872
• DSSTox Substance ID: DTXSID60306358
• Nikkaji Number: J2.169.492D
• Wikidata: Q82053421

Synonyms:1-(bromomethyl)cyclohexan-1-ol;17299-10-4;1-(bromomethyl)cyclohexanol;NSC175872;bromomethylcyclohexanol;SCHEMBL8451680;1-(bromomethyl)-cyclohexan-1-ol;DTXSID60306358;SSULDURTLPHCSZ-UHFFFAOYSA-N;1-hydroxy-1-bromomethyl cyclohexane;AKOS015906875;AB91237;NSC-175872;EN300-264957;F8884-9180

Chemical Property of 1-(Bromomethyl)cyclohexan-1-ol

Chemical Property:

• Vapor Pressure: 0.00555mmHg at 25°C
• Boiling Point: 243.1°Cat760mmHg
• Flash Point: 100.8°C
• Density: 1.418g/cm³
• XLogP3: 1.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 192.01498
• Heavy Atom Count: 9
• Complexity: 86.9

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC(CC1)(CBr)O

Technology Process of 1-(Bromomethyl)cyclohexan-1-ol

There total 5 articles about 1-(Bromomethyl)cyclohexan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + 1,1-dibromomethane (74-95-3) → 1-bromomethyl-1-cyclohexanol (17299-10-4)

Guidance literature:

1,1-dibromomethane; With titanium tetrachloride; magnesium; at 0 ℃; for 0.0166667h; Inert atmosphere;

cyclohexanone; In 1,2-dimethoxyethane; 1,2-dichloro-ethane; at 0 ℃; for 3h; Inert atmosphere;

DOI:10.1002/ejoc.201801438

Reference yield: 84.0%

methylenecyclohexane (1192-37-6) → 1-bromomethyl-1-cyclohexanol (17299-10-4)

Guidance literature:

With N-Bromosuccinimide; water; In various solvent(s); at 27 ℃; for 2h;

DOI:10.1016/j.tetlet.2005.03.108

Reference yield: 40.0%

1-oxaspiro(2.5)octane (185-70-6) → 1-bromomethyl-1-cyclohexanol (17299-10-4)

Guidance literature:

With lithium perchlorate; ammonium bromide; In acetonitrile; at 65 ℃; for 46h;

DOI:10.1016/S0040-4020(01)92271-9

upstream raw materials:

1-oxaspiro(2.5)octane

methylenecyclohexane

cyclohexanone

1,1-dibromomethane

Downstream raw materials:

1-(bromomethyl)-1-cyclohexyl chloroformate

1-(bromomethyl)-1-cyclohexyl phenylcarbamate

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