(Z)-2-Decene-4,6-diyneoic acid methyl ester

Base Information

• Chemical Name: (Z)-2-Decene-4,6-diyneoic acid methyl ester
• CAS No.: 505-01-1
• Molecular Formula: C11H12O2
• Molecular Weight: 176.215
• Mol file: 505-01-1.mol

Synonyms:cis-Lachnophyllum ester;Lachnophyllum ester;LACHNOPHYLLUM ESTER,CIS;cis-Lachnophyllummethylester;lachnophyllum methyl ester;methyl 2-cis-lachnophyllate;

Chemical Property of (Z)-2-Decene-4,6-diyneoic acid methyl ester

Chemical Property:

• Vapor Pressure: 0.00516mmHg at 25°C
• Boiling Point: 275.2°Cat760mmHg
• Flash Point: 110°C
• PSA: 26.30000
• Density: 1.013g/cm³
• LogP: 1.52250

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (Z)-2-Decene-4,6-diyneoic acid methyl ester

There total 7 articles about (Z)-2-Decene-4,6-diyneoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-2-decen-4,6-diynoic acid (80994-68-9) → methyl (Z)-dec-2-ene-4,6-diynoate (505-01-1,54497-59-5)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂SO₄

2: light petroleum / Irradiation

With sulfuric acid; In Petroleum ether;

DOI:10.1039/jr9630005759

Reference yield:

trans-lachnophyllum ester (3788-06-5,54497-59-5) → methyl (Z)-dec-2-ene-4,6-diynoate (505-01-1,54497-59-5)

Guidance literature:

In Petroleum ether; Irradiation;

DOI:10.1039/jr9630005759

Reference yield:

1-Pentyne (627-19-0) → methyl (Z)-dec-2-ene-4,6-diynoate (505-01-1,54497-59-5)

Guidance literature:

Multi-step reaction with 4 steps

1: ammonium chloride; copper (I)-chloride; aqueous hydrogen peroxide / Reagens₄: Wasser

2: manganese (IV)-oxide; dichloromethane

3: chromium (VI)-oxide; acetone; aqueous sulfuric acid

4: diethyl ether

With chromium(VI) oxide; manganese(IV) oxide; diethyl ether; dichloromethane; sulfuric acid; ammonium chloride; dihydrogen peroxide; acetone; copper(l) chloride;

upstream raw materials:

diazomethane

dec-2c-ene-4,6-diynoic acid

trans-lachnophyllum ester

1-Pentyne

Downstream raw materials:

oxalic acid

butyric acid

valeric acid

n-hexan-2-one