(4,5-Dimethoxy-2-nitrophenyl)(5-methylfuran-2-yl)methanone

Base Information

Chemical Name:(4,5-Dimethoxy-2-nitrophenyl)(5-methylfuran-2-yl)methanone
CAS No.:676546-91-1
Molecular Formula:C14H13NO6
Molecular Weight:291.25600
Hs Code.:
DSSTox Substance ID:DTXSID30428298
Wikidata:Q82241118
Mol file:676546-91-1.mol

Synonyms:676546-91-1;(4,5-Dimethoxy-2-nitrophenyl)(5-methylfuran-2-yl)methanone;DTXSID30428298;(4,5-Dimethoxy-2-nitro-phenyl)-(5-methyl-furan-2-yl)-methanone;Methanone, (4,5-dimethoxy-2-nitrophenyl)(5-methyl-2-furanyl)-;SB62001

Suppliers and Price of (4,5-Dimethoxy-2-nitrophenyl)(5-methylfuran-2-yl)methanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
(4,5-Dimethoxy-2-nitrophenyl)(5-methylfuran-2-yl)methanone 97%
1g
$ 617.00

Total 2 raw suppliers

Chemical Property of (4,5-Dimethoxy-2-nitrophenyl)(5-methylfuran-2-yl)methanone

Chemical Property:

PSA：94.49000
LogP:3.26760
XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:4
Exact Mass:291.07428713
Heavy Atom Count:21
Complexity:395

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

(4,5-Dimethoxy-2-nitrophenyl)(5-methylfuran-2-yl)methanone 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(O1)C(=O)C2=CC(=C(C=C2[N+](=O)[O-])OC)OC

Technology Process of (4,5-Dimethoxy-2-nitrophenyl)(5-methylfuran-2-yl)methanone

There total 3 articles about (4,5-Dimethoxy-2-nitrophenyl)(5-methylfuran-2-yl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 677299-77-3
(3,4-dimethoxy-phenyl)-(5-methyl-furan-2-yl)-methanone

: 676546-91-1
(4,5-dimethoxy-2-nitrophenyl)-(5-methyl-2-furyl)-methanone

Guidance literature:: With nitric acid; acetic acid; at 0 - 20 ℃; for 0.5h;
DOI:10.1016/j.tet.2006.10.056

Reference yield:

: 14003-11-3
5-methylfuran-2-carbonyl chloride

: 676546-91-1
(4,5-dimethoxy-2-nitrophenyl)-(5-methyl-2-furyl)-methanone

Guidance literature:: Multi-step reaction with 2 steps

1: AlCl₃ / benzene / 2.5 h / 55 - 60 °C

2: 65 percent / HNO₃; AcOH / 0.5 h / 0 - 20 °C

With aluminium trichloride; nitric acid; acetic acid; In benzene; 1: Friedel-Crafts reaction;
DOI:10.1016/j.tet.2006.10.056

Reference yield:

: 91-16-7
1,2-dimethoxybenzene

: 676546-91-1
(4,5-dimethoxy-2-nitrophenyl)-(5-methyl-2-furyl)-methanone

Guidance literature:: Multi-step reaction with 2 steps

1: AlCl₃ / benzene / 2.5 h / 55 - 60 °C

2: 65 percent / HNO₃; AcOH / 0.5 h / 0 - 20 °C

With aluminium trichloride; nitric acid; acetic acid; In benzene; 1: Friedel-Crafts reaction;
DOI:10.1016/j.tet.2006.10.056