N'-anilino-N-[4-[4-[[(E)-N-anilino-C-phenylcarbonimidoyl]diazenyl]phenyl]phenyl]iminobenzenecarboximidamide

Base Information

• Chemical Name: N'-anilino-N-[4-[4-[[(E)-N-anilino-C-phenylcarbonimidoyl]diazenyl]phenyl]phenyl]iminobenzenecarboximidamide
• CAS No.: 23305-70-6
• Molecular Formula: C38H30 N8
• Molecular Weight: 598.71
• NSC Number: 242017
• DSSTox Substance ID: DTXSID70422179
• Mol file: 23305-70-6.mol

Synonyms:NSC242017;23305-70-6;DTXSID70422179;21520-87-6;NSC-242017

Chemical Property of N'-anilino-N-[4-[4-[[(E)-N-anilino-C-phenylcarbonimidoyl]diazenyl]phenyl]phenyl]iminobenzenecarboximidamide

Chemical Property:

• Boiling Point: 748.7°Cat760mmHg
• Flash Point: 406.6°C
• Density: 1.17g/cm³
• XLogP3: 11.2
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 11
• Exact Mass: 598.25934299
• Heavy Atom Count: 46
• Complexity: 902

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=NNC2=CC=CC=C2)N=NC3=CC=C(C=C3)C4=CC=C(C=C4)N=NC(=NNC5=CC=CC=C5)C6=CC=CC=C6
• Isomeric SMILES: C1=CC=C(C=C1)/C(=N\NC2=CC=CC=C2)/N=NC3=CC=C(C=C3)C4=CC=C(C=C4)N=N/C(=N/NC5=CC=CC=C5)/C6=CC=CC=C6

Technology Process of N'-anilino-N-[4-[4-[[(E)-N-anilino-C-phenylcarbonimidoyl]diazenyl]phenyl]phenyl]iminobenzenecarboximidamide

There total 4 articles about N'-anilino-N-[4-[4-[[(E)-N-anilino-C-phenylcarbonimidoyl]diazenyl]phenyl]phenyl]iminobenzenecarboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.8%

p,p'-diaminobiphenyl (92-87-5) + benzaldehyde phenylhydrazone (588-64-7) → 1,1′-([1,1′-biphenyl]-4,4′-diyl)bis(3,5-diphenylformazan) (23305-70-6)

Guidance literature:

p,p'-diaminobiphenyl; With hydrogenchloride; sodium nitrite; In water;

benzaldehyde phenylhydrazone; With sodium hydroxide; In methanol; water; at 0 - 5 ℃; for 27h;

DOI:10.1134/S1070428021100055

Reference yield:

benzaldehyde (100-52-7) → 1,1′-([1,1′-biphenyl]-4,4′-diyl)bis(3,5-diphenylformazan) (23305-70-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium acetate / 1,4-dioxane; water / 20 °C

2.1: sodium nitrite; hydrogenchloride / water

2.2: 27 h / 0 - 5 °C

With hydrogenchloride; sodium acetate; sodium nitrite; In 1,4-dioxane; water;

DOI:10.1134/S1070428021100055

Reference yield:

phenyl-phenylhydrazono-acetic acid (728-95-0) → 3,5,3',5'-Tetraphenyl-1,1'-biphenyl-4,4'-diyl-di-formazan (23305-70-6)

Guidance literature:

With pyridine; ethanol;

DOI:10.1002/hlca.19540370102

upstream raw materials:

p,p'-diaminobiphenyl

benzaldehyde phenylhydrazone

benzaldehyde

phenyl-phenylhydrazono-acetic acid

Downstream raw materials:

3,3'-(4,4'-biphenylene)bis(2,5-diphenyl-2H-tetrazolium chloride)