1-(5-METHYL-FURAN-2-CARBONYL)-PIPERIDINE-2-CARBOXYLIC ACID

Base Information

• Chemical Name: 1-(5-METHYL-FURAN-2-CARBONYL)-PIPERIDINE-2-CARBOXYLIC ACID
• CAS No.: 427882-96-0
• Molecular Formula: C₁₂H₁₅NO₄
• Molecular Weight: 237.255
• Hs Code.: 2934999090
• Mol file: 427882-96-0.mol

Synonyms:1-(5-METHYL-FURAN-2-CARBONYL)-PIPERIDINE-2-CARBOXYLIC ACID

Chemical Property of 1-(5-METHYL-FURAN-2-CARBONYL)-PIPERIDINE-2-CARBOXYLIC ACID

Chemical Property:

• Vapor Pressure: 1.09E-08mmHg at 25°C
• Boiling Point: 444.7°Cat760mmHg
• Flash Point: 222.7°C
• PSA: 70.75000
• Density: g/cm³
• LogP: 1.60520

Purity/Quality:

97% ^*data from raw suppliers

1-(5-Methyl-furan-2-carbonyl)-piperidine-2-carboxylic acid ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(5-METHYL-FURAN-2-CARBONYL)-PIPERIDINE-2-CARBOXYLIC ACID

There total 4 articles about 1-(5-METHYL-FURAN-2-CARBONYL)-PIPERIDINE-2-CARBOXYLIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

5-methylfuran-2-carbonyl chloride (14003-11-3) + pipecolic Acid (4043-87-2,83680-83-5) → N-(5-methyl-2-furoyl)pipecolinic acid (427882-96-0)

Guidance literature:

With potassium hydroxide; In water; acetone; pH=9 - 10;

DOI:10.1023/A:1013926624228

Reference yield:

1-(5-methyl-furan-2-carbonyl)-piperidine-2-carboxylic acid methyl ester → N-(5-methyl-2-furoyl)pipecolinic acid (427882-96-0)

Guidance literature:

With potassium hydroxide; In ethanol; water; at 20 ℃;

DOI:10.1023/A:1013926624228

Reference yield:

5-methylfuran-2-carbonyl chloride (14003-11-3) → N-(5-methyl-2-furoyl)pipecolinic acid (427882-96-0)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / CHCl₃ / -2 - 20 °C

2: potassium hydroxide / H₂O; ethanol / 20 °C

With potassium hydroxide; triethylamine; In ethanol; chloroform; water;

DOI:10.1023/A:1013926624228

upstream raw materials:

5-methylfuran-2-carbonyl chloride

pipecolic Acid

methyl piperidine-2-carboxylate hydrochloride

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