4-(Dimethylsulfamoyl)benzene-1-sulfonyl chloride

Base Information

Chemical Name:4-(Dimethylsulfamoyl)benzene-1-sulfonyl chloride
CAS No.:677782-39-7
Molecular Formula:C₈H₁₀ClNO₄S₂
Molecular Weight:283.757
Hs Code.:
European Community (EC) Number:815-582-9
Mol file:677782-39-7.mol

Synonyms:4-(dimethylsulfamoyl)benzene-1-sulfonyl chloride;677782-39-7;4-(dimethylsulfamoyl)benzenesulfonyl Chloride;4-[(dimethylamino)sulfonyl]benzenesulfonyl chloride;SCHEMBL21244024;MFCD06340105;AKOS000200166;SB82168;BS-14048;CS-0139138;EN300-09889;4-(dimethylsulfamoyl)benzene-1-sulfonylchloride;C77555;4-(N,N-dimethylsulfamoyl)benzenesulfonyl chloride;A915462;Z56995197;Benzenesulfonyl chloride, 4-[(dimethylamino)sulfonyl]-;4-[(dimethylamino)sulfonyl]benzenesulfonyl chloride, AldrichCPR

Suppliers and Price of 4-(Dimethylsulfamoyl)benzene-1-sulfonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
4-(Dimethylsulfamoyl)benzene-1-sulfonylchloride 95+%
1g
$ 564.00

AK Scientific
4-(Dimethylsulfamoyl)benzene-1-sulfonylchloride
250mg
$ 340.00

Total 3 raw suppliers

Chemical Property of 4-(Dimethylsulfamoyl)benzene-1-sulfonyl chloride

Chemical Property:

XLogP3:1.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:282.9739778
Heavy Atom Count:16
Complexity:424

Purity/Quality:

97% ^*data from raw suppliers

4-(Dimethylsulfamoyl)benzene-1-sulfonylchloride 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(C)S(=O)(=O)C1=CC=C(C=C1)S(=O)(=O)Cl

Technology Process of 4-(Dimethylsulfamoyl)benzene-1-sulfonyl chloride

There total 3 articles about 4-(Dimethylsulfamoyl)benzene-1-sulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18325-52-5
4-mercapto-N,N-dimethylbenzenesulfonamide

: 677782-39-7
4-(N,N-dimethylsulfamoyl)benzene-1-sulfonyl chloride

Guidance literature:: With hydrogenchloride; In dichloromethane; water; at 0 - 5 ℃; for 0.5h;

Reference yield:

: 98-58-8
4-bromobenzenesulfonyl chloride

: 677782-39-7
4-(N,N-dimethylsulfamoyl)benzene-1-sulfonyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 2 h / 5 - 20 °C

2.1: isopropylmagnesium chloride; n-butyllithium / tetrahydrofuran / 0.75 h / -10 °C / Inert atmosphere

2.2: 1 h / -20 - -10 °C

3.1: hydrogenchloride / dichloromethane; water / 0.5 h / 0 - 5 °C

With hydrogenchloride; n-butyllithium; isopropylmagnesium chloride; triethylamine; In tetrahydrofuran; dichloromethane; water;

Reference yield:

: 707-60-8
4-bromo-N,N-dimethylbenzenesulfonamide

: 677782-39-7
4-(N,N-dimethylsulfamoyl)benzene-1-sulfonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: isopropylmagnesium chloride; n-butyllithium / tetrahydrofuran / 0.75 h / -10 °C / Inert atmosphere

1.2: 1 h / -20 - -10 °C

2.1: hydrogenchloride / dichloromethane; water / 0.5 h / 0 - 5 °C

With hydrogenchloride; n-butyllithium; isopropylmagnesium chloride; In tetrahydrofuran; dichloromethane; water;