(2,2-Dimethoxyethyl)(diphenyl)phosphane

Base Information

Chemical Name:(2,2-Dimethoxyethyl)(diphenyl)phosphane
CAS No.:24744-62-5
Molecular Formula:C16H19 O2 P
Molecular Weight:274.299
Hs Code.:
NSC Number:132581
DSSTox Substance ID:DTXSID30299768
Nikkaji Number:J1.217.808E
Wikidata:Q82042415
Mol file:24744-62-5.mol

Synonyms:24744-62-5;(2,2-dimethoxyethyl)(diphenyl)phosphane;NSC132581;DTXSID30299768;NSC-132581

Suppliers and Price of (2,2-Dimethoxyethyl)(diphenyl)phosphane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of (2,2-Dimethoxyethyl)(diphenyl)phosphane

Chemical Property:

Vapor Pressure:5.64E-05mmHg at 25°C
Boiling Point:357.4°Cat760mmHg
Flash Point:208.7°C
Density:g/cm³
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:274.11226684
Heavy Atom Count:19
Complexity:213

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC(CP(C1=CC=CC=C1)C2=CC=CC=C2)OC

Technology Process of (2,2-Dimethoxyethyl)(diphenyl)phosphane

There total 6 articles about (2,2-Dimethoxyethyl)(diphenyl)phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 97-97-2
chloroacetaldehyde dimethyl acetal

: 15475-27-1,4346-39-8
potassium diphenylphosphine

: 24744-62-5
(diphenylphosphino)acetaldehyde dimethyl acetal

Guidance literature:: In tetrahydrofuran; at 0 - 20 ℃; for 3h; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.molstruc.2016.12.023

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 24744-62-5
(diphenylphosphino)acetaldehyde dimethyl acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / diethyl ether / overnight

2: hydroquinone / acetonitrile / 80 h / 60 - 70 °C / argon-filled sealed ampul

3: H₂O, KCN / 4 h / Heating

With potassium cyanide; water; hydroquinone; In diethyl ether; acetonitrile;

Reference yield:

: 2741-38-0
allyldiphenylphosphine

: 24744-62-5
(diphenylphosphino)acetaldehyde dimethyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: hydroquinone / acetonitrile / 80 h / 60 - 70 °C / argon-filled sealed ampul

2: H₂O, KCN / 4 h / Heating

With potassium cyanide; water; hydroquinone; In acetonitrile;