1-(3,7-Dinitro-10h-phenothiazin-10-yl)ethanone

Base Information

Chemical Name:1-(3,7-Dinitro-10h-phenothiazin-10-yl)ethanone
CAS No.:1628-79-1
Molecular Formula:C₁₄H₉N₃O₅S
Molecular Weight:331.309
Hs Code.:
NSC Number:95823
DSSTox Substance ID:DTXSID40294325
Wikidata:Q82033572
Mol file:1628-79-1.mol

Synonyms:1628-79-1;1-(3,7-dinitro-10h-phenothiazin-10-yl)ethanone;NSC95823;SCHEMBL1208152;DTXSID40294325;VUWDHXCPXJCIJQ-UHFFFAOYSA-N;10-acetyl-3,7-dinitrophenothiazine;3,7-dinitro-10-acetylphenothiazine;NSC-95823;3,7-Dinitro-10-acetyl-phenothiazine;1-(3,7-dinitro-phenothiazin-10-yl)-ethanone

Suppliers and Price of 1-(3,7-Dinitro-10h-phenothiazin-10-yl)ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 1-(3,7-Dinitro-10h-phenothiazin-10-yl)ethanone

Chemical Property:

Vapor Pressure:1.09E-16mmHg at 25°C
Boiling Point:648.2°Cat760mmHg
Flash Point:345.8°C
Density:1.566g/cm³
XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:0
Exact Mass:331.02629157
Heavy Atom Count:23
Complexity:482

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)N1C2=C(C=C(C=C2)[N+](=O)[O-])SC3=C1C=CC(=C3)[N+](=O)[O-]

Technology Process of 1-(3,7-Dinitro-10h-phenothiazin-10-yl)ethanone

There total 4 articles about 1-(3,7-Dinitro-10h-phenothiazin-10-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1747-90-6
3,11-dinitro-10H-phenothiazine

: 108-24-7
acetic anhydride

: 1628-79-1
1-(3,7-dinitrophenothiazin-10-yl)-ethanone

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 105 ℃; for 3h;

Reference yield:

: 92-84-2
10H-phenothiazine

: 1628-79-1
1-(3,7-dinitrophenothiazin-10-yl)-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: sodium nitrite; acetic acid / dimethyl sulfoxide / 19 h / 20 - 95 °C

2: triethylamine / N,N-dimethyl-formamide / 3 h / 105 °C

With acetic acid; triethylamine; sodium nitrite; In dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 1628-77-9
3-nitro-10H-phenothiazine

: 1628-79-1
1-(3,7-dinitrophenothiazin-10-yl)-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; sodium nitrite / chloroform / 20 °C

2: pyridine / 18 h / Heating / reflux

With pyridine; acetic acid; sodium nitrite; In chloroform;