Technology Process of Anziaic acid
There total 9 articles about Anziaic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
ethyl acetate;
at 20 ℃;
for 2h;
under 750.075 Torr;
DOI:10.1039/c3md00238a
- Guidance literature:
-
Multi-step reaction with 5 steps
1: trichlorophosphate / 18 h / 0 - 20 °C
2: potassium carbonate / acetone / 12 h / Reflux
3: sodium dihydrogenphosphate; sodium chlorite / dimethyl sulfoxide; water / 14 h / 20 °C
4: trifluoroacetic anhydride / toluene / 20 °C
5: palladium 10% on activated carbon; hydrogen / ethyl acetate / 2 h / 20 °C / 750.08 Torr
With
sodium chlorite; sodium dihydrogenphosphate; palladium 10% on activated carbon; hydrogen; potassium carbonate; trifluoroacetic anhydride; trichlorophosphate;
In
water; dimethyl sulfoxide; ethyl acetate; acetone; toluene;
1: |Vilsmeier-Haack Formylation;
DOI:10.1039/c3md00238a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium dihydrogenphosphate; sodium chlorite / dimethyl sulfoxide; water / 14 h / 0 - 20 °C
2: potassium hydrogencarbonate / N,N-dimethyl-formamide / 5 h / 20 °C
3: trifluoroacetic anhydride / toluene / 20 °C
4: palladium 10% on activated carbon; hydrogen / ethyl acetate / 2 h / 20 °C / 750.08 Torr
With
sodium chlorite; sodium dihydrogenphosphate; palladium 10% on activated carbon; hydrogen; potassium hydrogencarbonate; trifluoroacetic anhydride;
In
water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1039/c3md00238a
