2-chloro-N-(2-chloroethyl)-N-[(3,4-dichlorophenyl)methyl]ethanamine;hydrochloride

Base Information

• Chemical Name: 2-chloro-N-(2-chloroethyl)-N-[(3,4-dichlorophenyl)methyl]ethanamine;hydrochloride
• CAS No.: 60855-83-6
• Molecular Formula: C11H13Cl4N
• Molecular Weight: 337.504
• DSSTox Substance ID: DTXSID20489732
• NSC Number: 53915

Synonyms:60855-83-6;DTXSID20489732;NSC53915;NSC-53915;2-Chloro-N-(2-chloroethyl)-N-[(3,4-dichlorophenyl)methyl]ethan-1-amine--hydrogen chloride (1/1)

Chemical Property of 2-chloro-N-(2-chloroethyl)-N-[(3,4-dichlorophenyl)methyl]ethanamine;hydrochloride

Chemical Property:

• Vapor Pressure: 0.00103mmHg at 25°C
• Boiling Point: 301.8°Cat760mmHg
• Flash Point: 136.3°C
• Density: 1.333g/cm³
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 6
• Exact Mass: 336.953938
• Heavy Atom Count: 17
• Complexity: 185

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C=C1CN(CCCl)CCCl)Cl)Cl.Cl

Technology Process of 2-chloro-N-(2-chloroethyl)-N-[(3,4-dichlorophenyl)methyl]ethanamine;hydrochloride

There total 1 articles about 2-chloro-N-(2-chloroethyl)-N-[(3,4-dichlorophenyl)methyl]ethanamine;hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2-[(2-hydroxyethyl)(3,4-dichlorobenzyl)amino]ethanol hydrochloride → (3,4-dichlorobenzyl)-bis(2-chloroethyl)amine hydrochloride (60855-83-6)

Guidance literature:

With thionyl chloride; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1021/jm0205550

Reference yield: 60.0%

2-(4-methoxybenzenesulfonyl)acetic acid ethyl ester (2850-21-7) + (3,4-dichlorobenzyl)-bis(2-chloroethyl)amine hydrochloride (60855-83-6) → 1-(3,4-dichloro-benzyl)-4-(4-methoxy-benzenesulfonyl)-piperidine-4-carboxylic acid ethyl ester (212770-62-2)

Guidance literature:

With 18-crown-6 ether; potassium carbonate; In acetone; for 16h; Heating;

DOI:10.1021/jm0205550

Reference yield: 60.0%

(3,4-dichlorobenzyl)-bis(2-chloroethyl)amine hydrochloride (60855-83-6) + 4-(n-butoxy-benzenesulfonyl) acetic acid ethyl ester → 4-(4-butoxybenzenesulfonyl)-1-(3,4-dichlorobenzyl)piperidine-4-carboxylic acid ethyl ester (239798-27-7)

Guidance literature:

With 18-crown-6 ether; potassium carbonate; In acetone; for 16h; Heating;

DOI:10.1021/jm0205550

Downstream raw materials:

1-(3,4-dichloro-benzyl)-4-(4-methoxy-benzenesulfonyl)-piperidine-4-carboxylic acid ethyl ester

4-(4-butoxybenzenesulfonyl)-1-(3,4-dichlorobenzyl)piperidine-4-carboxylic acid ethyl ester

1-(3,4-dichloro-benzyl)-4-(4-methoxy-benzenesulfonyl)-piperidine-4-carboxylic acid

1-(3,4-dichlorobenzyl)-4-(4-butoxybenzenesulfonyl)piperidine-4-carboxylic acid

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 60855-83-6 2-chloro-N-(2-chloroethyl)-N-(3,4-dichlorobenzyl)ethanamine

Send

Send

Metric Ton KG G Pound L ML

Send

Send