Pyrrolo[2,1-a]isoquinoline-3-carboxylic acid, 2-(2,4-dihydroxy-5-methoxyphenyl)-5,6-dihydro-8-hydroxy-1-(3-hydroxy- 4-methoxyphenyl)-9-methoxy-, ethyl ester

Base Information

Chemical Name:Pyrrolo[2,1-a]isoquinoline-3-carboxylic acid, 2-(2,4-dihydroxy-5-methoxyphenyl)-5,6-dihydro-8-hydroxy-1-(3-hydroxy- 4-methoxyphenyl)-9-methoxy-, ethyl ester
CAS No.:680189-50-8
Molecular Formula:C30H29NO9
Molecular Weight:547.562
Hs Code.:

Pyrrolo[2,1-a]isoquinoline-3-carboxylic acid,
2-(2,4-dihydroxy-5-methoxyphenyl)-5,6-dihydro-8-hydroxy-1-(3-hydroxy-
4-methoxyphenyl)-9-methoxy-, ethyl ester

Synonyms:

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Chemical Property of Pyrrolo[2,1-a]isoquinoline-3-carboxylic acid, 2-(2,4-dihydroxy-5-methoxyphenyl)-5,6-dihydro-8-hydroxy-1-(3-hydroxy- 4-methoxyphenyl)-9-methoxy-, ethyl ester

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Technology Process of Pyrrolo[2,1-a]isoquinoline-3-carboxylic acid, 2-(2,4-dihydroxy-5-methoxyphenyl)-5,6-dihydro-8-hydroxy-1-(3-hydroxy- 4-methoxyphenyl)-9-methoxy-, ethyl ester

There total 22 articles about Pyrrolo[2,1-a]isoquinoline-3-carboxylic acid, 2-(2,4-dihydroxy-5-methoxyphenyl)-5,6-dihydro-8-hydroxy-1-(3-hydroxy- 4-methoxyphenyl)-9-methoxy-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 680189-48-4
ethyl 8-(benzyloxy)-1-(3-(benzyloxy)-4-methoxyphenyl)-2-(2,4-bis(benzyloxy)-5-methoxyphenyl)-9-methoxy-5,6-dihydropyrrolo-[2,1-a]isoquinoline-3-carboxylate

: 680189-50-8
2-(2,4-dihydroxy-5-methoxy-phenyl)-8-hydroxy-1-(3-hydroxy-4-methoxy-phenyl)-9-methoxy-5,6-dihydro-pyrrolo[2,1-a]isoquinoline-3-carboxylic acid ethyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate;
DOI:10.1002/anie.200352043

Reference yield:

: 21411-27-8
6-(benzyloxy)-1-[3-(benzyloxy)-4-methoxybenzyl]-7-methoxy-3,4-dihydroisoquinoline

: 680189-50-8
2-(2,4-dihydroxy-5-methoxy-phenyl)-8-hydroxy-1-(3-hydroxy-4-methoxy-phenyl)-9-methoxy-5,6-dihydro-pyrrolo[2,1-a]isoquinoline-3-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / NaHCO₃ / acetonitrile / Heating

2: 100 percent / H₂ / Pd/C / ethyl acetate

With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In ethyl acetate; acetonitrile;
DOI:10.1002/anie.200352043

Reference yield:

: 1034028-91-5
(Z)-ethyl 2,4-bis(benzyloxy)-5-methoxy-α-nitrocinnamate

: 680189-50-8
2-(2,4-dihydroxy-5-methoxy-phenyl)-8-hydroxy-1-(3-hydroxy-4-methoxy-phenyl)-9-methoxy-5,6-dihydro-pyrrolo[2,1-a]isoquinoline-3-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / NaHCO₃ / acetonitrile / Heating

2: 100 percent / H₂ / Pd/C / ethyl acetate

With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In ethyl acetate; acetonitrile;
DOI:10.1002/anie.200352043