1-(4-Phenylpiperazin-1-yl)ethanone

Base Information

• Chemical Name: 1-(4-Phenylpiperazin-1-yl)ethanone
• CAS No.: 21557-13-1
• Molecular Formula: C12H16N2O
• Molecular Weight: 204.272
• Hs Code.: 2933599090
• Mol file: 21557-13-1.mol

Synonyms:Ethanone, 1-(4-phenyl-1-piperazinyl)-;N-Acetyl-N'-phenylpiperazine;1-(4-Phenylpiperazino)ethan-1-one;1-Acetyl-4-phenylpiperazine;

Chemical Property of 1-(4-Phenylpiperazin-1-yl)ethanone

Chemical Property:

• Vapor Pressure: 8.57E-06mmHg at 25°C
• Melting Point: 92-94 °C
• Refractive Index: 1.556
• Boiling Point: 374.1 °C at 760 mmHg
• Flash Point: 171 °C
• PSA: 23.55000
• Density: 1.11 g/cm³
• LogP: 1.35800

Purity/Quality:

99% ^*data from raw suppliers

EV000198:1-(4-Phenyl-piperazin-1-yl)-ethanone 97 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(4-Phenylpiperazin-1-yl)ethanone

There total 15 articles about 1-(4-Phenylpiperazin-1-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-(4-acetylpiperazin-1-yl)phenyl diisopropylsulfamate → 1-(4-phenylpiperazin-1-yl)ethan-1-one (21557-13-1)

Guidance literature:

With potassium phosphate; 4,5-dimethyl-1,3-bis-(2,4,6-trimethylphenyl)-3H-imidazol-1-ium chloride; C₄₆H₃₉ClNiP₂; isopropyl alcohol; In toluene; at 80 ℃; for 15.15h;

DOI:10.1055/a-1548-8362

Reference yield: 99.0%

4-(4-acetylpiperazin-1-yl)phenyl diethylsulfamate → 1-(4-phenylpiperazin-1-yl)ethan-1-one (21557-13-1)

Guidance literature:

With potassium phosphate; 4,5-dimethyl-1,3-bis-(2,4,6-trimethylphenyl)-3H-imidazol-1-ium chloride; C₄₆H₃₉ClNiP₂; isopropyl alcohol; In toluene; at 80 ℃; for 15.15h;

DOI:10.1055/a-1548-8362

Reference yield: 99.0%

C14H21N3O4S → 1-(4-phenylpiperazin-1-yl)ethan-1-one (21557-13-1)

Guidance literature:

With potassium phosphate; 4,5-dimethyl-1,3-bis-(2,4,6-trimethylphenyl)-3H-imidazol-1-ium chloride; C₄₆H₃₉ClNiP₂; isopropyl alcohol; In toluene; at 80 ℃; for 15.15h;

DOI:10.1055/a-1548-8362

upstream raw materials:

4-phenyl-1-piperazine

acetic anhydride

acetyl chloride

bis(2-bromoethyl)amine hydrobromide

Downstream raw materials:

1-acetyl-4-(4-phenylazo-phenyl)-piperazine

1-{4-[4-(4-Trifluoromethyl-phenylazo)-phenyl]-piperazin-1-yl}-ethanone

4,5-Dimethoxy-2-[1-(4-phenyl-piperazin-1-yl)-eth-(E)-ylideneamino]-benzonitrile

1-{4-[4-(4-Chloro-phenylazo)-phenyl]-piperazin-1-yl}-ethanone

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