3,29-Dioxa-5,9,14,18-tetraazahentriacont-23-ene-21,25-diyne-9,14,18- tricarboxylic acid, 28-cyano-2,2-dimethyl-4,30-dioxo-28-phenyl-, tris(1,1-dimethylethyl) ester, (23Z)-

Base Information

Chemical Name:3,29-Dioxa-5,9,14,18-tetraazahentriacont-23-ene-21,25-diyne-9,14,18- tricarboxylic acid, 28-cyano-2,2-dimethyl-4,30-dioxo-28-phenyl-, tris(1,1-dimethylethyl) ester, (23Z)-
CAS No.:681124-12-9
Molecular Formula:C49H73N5O10
Molecular Weight:892.146
Hs Code.:

3,29-Dioxa-5,9,14,18-tetraazahentriacont-23-ene-21,25-diyne-9,14,18-
tricarboxylic acid, 28-cyano-2,2-dimethyl-4,30-dioxo-28-phenyl-,
tris(1,1-dimethylethyl) ester, (23Z)-

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Chemical Property of 3,29-Dioxa-5,9,14,18-tetraazahentriacont-23-ene-21,25-diyne-9,14,18- tricarboxylic acid, 28-cyano-2,2-dimethyl-4,30-dioxo-28-phenyl-, tris(1,1-dimethylethyl) ester, (23Z)-

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Technology Process of 3,29-Dioxa-5,9,14,18-tetraazahentriacont-23-ene-21,25-diyne-9,14,18- tricarboxylic acid, 28-cyano-2,2-dimethyl-4,30-dioxo-28-phenyl-, tris(1,1-dimethylethyl) ester, (23Z)-

There total 9 articles about 3,29-Dioxa-5,9,14,18-tetraazahentriacont-23-ene-21,25-diyne-9,14,18- tricarboxylic acid, 28-cyano-2,2-dimethyl-4,30-dioxo-28-phenyl-, tris(1,1-dimethylethyl) ester, (23Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 681124-02-7
Acetic acid (Z)-6-chloro-1-cyano-1-phenyl-hex-5-en-3-ynyl ester

: 681124-09-4
[3-(tert-butoxycarbonyl-{4-[tert-butoxycarbonyl-(3-tert-butoxycarbonylamino-propyl)-amino]-butyl}-amino)-propyl]-but-3-ynyl-carbamic acid tert-butyl ester

: 681124-12-9
acetic acid 10-{tert-butoxycarbonyl-[3-(tert-butoxycarbonyl-{4-[tert-butoxycarbonyl-(3-tert-butoxycarbonylamino-propyl)-amino]-butyl}-amino)-propyl]-amino}-1-cyano-1-phenyl-dec-5-ene-3,7-diynyl ester

Guidance literature:: With diethylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In benzene; at 20 ℃;
DOI:10.1016/j.tetlet.2003.12.139

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 681124-12-9
acetic acid 10-{tert-butoxycarbonyl-[3-(tert-butoxycarbonyl-{4-[tert-butoxycarbonyl-(3-tert-butoxycarbonylamino-propyl)-amino]-butyl}-amino)-propyl]-amino}-1-cyano-1-phenyl-dec-5-ene-3,7-diynyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH / dioxane / 20 °C

2: 68 percent / Et₂NH / Pd(PPh₃)4; CuI / benzene / 20 °C

With sodium hydroxide; diethylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; benzene; 2: Sonogashira coupling;
DOI:10.1016/j.tetlet.2003.12.139

Reference yield:

: 41865-47-8
2-<(2-tetrahydropyranyl)oxy>-2-phenylacetonitrile

: 681124-12-9
acetic acid 10-{tert-butoxycarbonyl-[3-(tert-butoxycarbonyl-{4-[tert-butoxycarbonyl-(3-tert-butoxycarbonylamino-propyl)-amino]-butyl}-amino)-propyl]-amino}-1-cyano-1-phenyl-dec-5-ene-3,7-diynyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 43 percent / LDA / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 °C

2: 96 percent / n-BuNH₂ / Pd(PPh₃)4; CuI / benzene / 20 °C

3: p-TsOH / methanol / 20 °C

4: EDC; DMAP / CH₂Cl₂ / 0 °C

5: 68 percent / Et₂NH / Pd(PPh₃)4; CuI / benzene / 20 °C

With dmap; toluene-4-sulfonic acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; diethylamine; N-butylamine; lithium diisopropyl amide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; benzene; 2: Sonogashira coupling / 5: Sonogashira coupling;
DOI:10.1016/j.tetlet.2003.12.139