2-Chloro-3-(N-ethylacetamido)-1,4-naphthoquinone

Base Information

Chemical Name:2-Chloro-3-(N-ethylacetamido)-1,4-naphthoquinone
CAS No.:4497-72-7
Molecular Formula:C14H12ClNO3
Molecular Weight:277.703
Hs Code.:
DSSTox Substance ID:DTXSID50196346
Wikidata:Q83069412

Synonyms:4497-72-7;2-Chloro-3-(N-ethylacetamido)-1,4-naphthoquinone;2-Chloro-3-[N-ethylacetamido]-1,4-naphthoquinone;DTXSID50196346;STL329053;AKOS022096995;SR-01000224671;SR-01000224671-1;1,4-Naphthoquinone, 2-(N-ethylacetamido)-3-chloro-;N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-N-ethylacetamide

Suppliers and Price of 2-Chloro-3-(N-ethylacetamido)-1,4-naphthoquinone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-Chloro-3-(N-ethylacetamido)-1,4-naphthoquinone

Chemical Property:

Vapor Pressure:7.94E-07mmHg at 25°C
Boiling Point:406.8°Cat760mmHg
Flash Point:199.8°C
Density:1.35g/cm³
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:277.0505709
Heavy Atom Count:19
Complexity:469

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(C1=C(C(=O)C2=CC=CC=C2C1=O)Cl)C(=O)C

Technology Process of 2-Chloro-3-(N-ethylacetamido)-1,4-naphthoquinone

There total 3 articles about 2-Chloro-3-(N-ethylacetamido)-1,4-naphthoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.9%

: 5349-87-1
2-chloro-3-(ethylamino)naphthalene-1,4-dione

: 108-24-7
acetic anhydride

: 4497-72-7
N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-N-ethylacetamide

Guidance literature:: With sulfuric acid; at 20 ℃; for 1.5h;
DOI:10.1016/j.ejmech.2015.09.026

Reference yield:

: 117-80-6
2,3-Dichloro-1,4-naphthoquinone

: 4497-72-7
N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-N-ethylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / ethanol / 18 h / 20 °C

2: sulfuric acid / 1.5 h / 20 °C

With sulfuric acid; triethylamine; In ethanol;
DOI:10.1016/j.ejmech.2015.09.026