Benzoic acid, 2,6-bis(trifluoromethyl)-, 3-[[(2S)-2-amino-1-oxo-3-phenylpropyl]amino]-2-oxopropyl ester, mono(4-methylbenzenesulfonate)

Base Information

Chemical Name:Benzoic acid, 2,6-bis(trifluoromethyl)-, 3-[[(2S)-2-amino-1-oxo-3-phenylpropyl]amino]-2-oxopropyl ester, mono(4-methylbenzenesulfonate)
CAS No.:681447-88-1
Molecular Formula:C21H18F6N2O4.C7H8O3S
Molecular Weight:648.58
Hs Code.:

Benzoic acid, 2,6-bis(trifluoromethyl)-,
3-[[(2S)-2-amino-1-oxo-3-phenylpropyl]amino]-2-oxopropyl ester,
mono(4-methylbenzenesulfonate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 2,6-bis(trifluoromethyl)-, 3-[[(2S)-2-amino-1-oxo-3-phenylpropyl]amino]-2-oxopropyl ester, mono(4-methylbenzenesulfonate)

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Technology Process of Benzoic acid, 2,6-bis(trifluoromethyl)-, 3-[[(2S)-2-amino-1-oxo-3-phenylpropyl]amino]-2-oxopropyl ester, mono(4-methylbenzenesulfonate)

There total 1 articles about Benzoic acid, 2,6-bis(trifluoromethyl)-, 3-[[(2S)-2-amino-1-oxo-3-phenylpropyl]amino]-2-oxopropyl ester, mono(4-methylbenzenesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: C₂₉H₂₄F₆N₂O₆

: 104-15-4
toluene-4-sulfonic acid

: 681447-88-1
2,6-bis-trifluoromethyl-benzoic acid-3-(2-amino-3-phenyl-propionylamino)-2-oxo-propyl ester p-toluenesulfonic acid salt

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In methanol; at 20 ℃; for 1.5h;

Reference yield: 24.0%

: 681447-88-1
2,6-bis-trifluoromethyl-benzoic acid-3-(2-amino-3-phenyl-propionylamino)-2-oxo-propyl ester p-toluenesulfonic acid salt

: 10436-25-6
11-(tert-butoxycarbonylamino)undecanoic acid

: 681447-89-2
2,6-bis-trifluoromethyl-benzoic acid 3-[2-(11-tert-butoxycarbonylamino-10-methyl-undecanoylamino)-3-phenyl-propionylamino]-2-oxo-propyl ester

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In DMF (N,N-dimethyl-formamide); for 18h;