1-Azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid, 3-[(diphenoxyphosphinyl)oxy]-6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-, (2,2-dimethyl-1-oxopropoxy)methyl ester, (4R,5R,6S)-

Base Information

Chemical Name:1-Azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid, 3-[(diphenoxyphosphinyl)oxy]-6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-, (2,2-dimethyl-1-oxopropoxy)methyl ester, (4R,5R,6S)-
CAS No.:682747-73-5
Molecular Formula:C28H32NO10P
Molecular Weight:573.537
Hs Code.:

1-Azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid,
3-[(diphenoxyphosphinyl)oxy]-6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-,
(2,2-dimethyl-1-oxopropoxy)methyl ester, (4R,5R,6S)-

Synonyms:

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Chemical Property of 1-Azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid, 3-[(diphenoxyphosphinyl)oxy]-6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-, (2,2-dimethyl-1-oxopropoxy)methyl ester, (4R,5R,6S)-

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Technology Process of 1-Azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid, 3-[(diphenoxyphosphinyl)oxy]-6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-, (2,2-dimethyl-1-oxopropoxy)methyl ester, (4R,5R,6S)-

There total 4 articles about 1-Azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid, 3-[(diphenoxyphosphinyl)oxy]-6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-, (2,2-dimethyl-1-oxopropoxy)methyl ester, (4R,5R,6S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 692779-24-1
(4R,5R,6S)-6-[(1R)-1-trimethylsilyloxyethyl]-3-diphenylphosphoryloxy-4-methyl-7-oxo-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid pivaloyloxymethyl ester

: 682747-73-5
(4R,SR,6S)-6-[(1R)-1-hydroxyethyl]-3-diphenylphosphoryloxy-4-methyl-7-oxo-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid pivaloyloxymethyl ester

Guidance literature:: With hydrogenchloride; water; In tetrahydrofuran; ethyl acetate; toluene; pH=3;

Reference yield:

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 682747-73-5
(4R,SR,6S)-6-[(1R)-1-hydroxyethyl]-3-diphenylphosphoryloxy-4-methyl-7-oxo-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid pivaloyloxymethyl ester

Guidance literature:: C₂₅H₃₆ClNO₇SSi; With potassium tert-butylate; In tetrahydrofuran; toluene; at -25 ℃; for 1h;

With methyl iodide; In tetrahydrofuran; toluene; at -25 ℃; for 0.333333h;

chlorophosphoric acid diphenyl ester; With hydrogenchloride; water; more than 3 stages; Product distribution / selectivity;

Reference yield:

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 682747-73-5
(4R,SR,6S)-6-[(1R)-1-hydroxyethyl]-3-diphenylphosphoryloxy-4-methyl-7-oxo-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid pivaloyloxymethyl ester

: 692779-24-1
(4R,5R,6S)-6-[(1R)-1-trimethylsilyloxyethyl]-3-diphenylphosphoryloxy-4-methyl-7-oxo-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid pivaloyloxymethyl ester

Guidance literature:: C₂₅H₃₆ClNO₇SSi; With potassium tert-butylate; In tetrahydrofuran; at -70 ℃; for 0.25h;

With methyl iodide; In tetrahydrofuran; at -70 - -35 ℃; for 0.416667h;

chlorophosphoric acid diphenyl ester; With water; more than 3 stages; Product distribution / selectivity;