Benzoic acid, 4,4',4'',4'''-stannanetetrayltetrakis-

Base Information

Chemical Name:Benzoic acid, 4,4',4'',4'''-stannanetetrayltetrakis-
CAS No.:684237-26-1
Molecular Formula:C₂₈H₂₀O₈Sn
Molecular Weight:603.172
Hs Code.:

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Chemical Property of Benzoic acid, 4,4',4'',4'''-stannanetetrayltetrakis-

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Technology Process of Benzoic acid, 4,4',4'',4'''-stannanetetrayltetrakis-

There total 1 articles about Benzoic acid, 4,4',4'',4'''-stannanetetrayltetrakis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 107386-98-1
Sn(C₆H₄CHO)4

: 7722-84-1
dihydrogen peroxide

: 684237-26-1
Sn(C₆H₄COOH)4

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; In tetrahydrofuran; water; soln. of NaH2PO4 in H2O and aq. soln. of H2O2 added to soln. of Sn compd. in THF; refluxed for 5 min; NaClO2 in H2O added over 30 min; stirred at room temp. overnight; THF evapd.; diluted with water; extd. with CH2Cl2; org. layer stored over anhyd. MgSO4; concd.; dried in vac.; elem. anal.;
DOI:10.1016/j.jorganchem.2004.02.012

Reference yield: 50.0%

: 684237-26-1
Sn(C₆H₄COOH)4

: 616-34-2
methoxycarbonylmethylamine

: 684237-29-4
Sn(C₆H₄CONHCH₂COOCH₃)4

Guidance literature:: With benzotriazol-1-ol; triethylamine; In tetrahydrofuran; byproducts: H2O; Sn compd. dissolved in THF; H2NCH2COOMe, Et3N and 1-hydroxybenzotriazoleadded at 0°C, pH 5; diisopropyldiimide added; stirred at 0.degre e.C for 30 min; warmed to room temp. overnight; filtered; vac. dried;
DOI:10.1016/j.jorganchem.2004.02.012