Tris(acetyloxy)(2-methoxyphenyl)plumbane

Base Information Edit

Chemical Name:Tris(acetyloxy)(2-methoxyphenyl)plumbane
CAS No.:68490-98-2
Molecular Formula:C13H16O7Pb
Molecular Weight:491.466
Hs Code.:
DSSTox Substance ID:DTXSID10586880
Wikidata:Q82479102
Mol file:68490-98-2.mol

Synonyms:68490-98-2;Tris(acetyloxy)(2-methoxyphenyl)plumbane;DTXSID10586880

Suppliers and Price of Tris(acetyloxy)(2-methoxyphenyl)plumbane

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Tris(acetyloxy)(2-methoxyphenyl)plumbane Edit

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:8
Exact Mass:492.06625
Heavy Atom Count:21
Complexity:369

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)O[Pb](C1=CC=CC=C1OC)(OC(=O)C)OC(=O)C

Technology Process of Tris(acetyloxy)(2-methoxyphenyl)plumbane

There total 2 articles about Tris(acetyloxy)(2-methoxyphenyl)plumbane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: lead(IV) acetate

: 86487-17-4
2-tri-n-butylstannylanisole

: 68490-98-2
o-Methoxyphenyllead(IV) triacetate

Guidance literature:: mercury(II) trifluoroacetate; In chloroform; byproducts: Bu3SnOAc; stirred at 40°C for 2 h;; filtered through Celite; solvent removed; light petroleum added; ppt. washed with light petroleum; crystd. from CHCl3/light petroleum; elem. anal.;;

Reference yield: 88.0%

: lead(IV) tetraacetate

: 13257-51-7
mercury(II) trifluoroacetate

: 86487-17-4
2-tri-n-butylstannylanisole

: 68490-98-2
C₆H₄(OCH₃)Pb(OOCCH₃)3

Guidance literature:: In chloroform; addn. of Sn-compd. and Hg(OOCCF3) to a soln. of Pb(OAc)4 in CHCl3, stirring at 40°C overnight; filtration (Kieselgur), evapn. of filtrate (vac., 40°C), dissoln. of oily residue in petroleum ether (40-60°C), crystn. on storing in refrigerator, recrystn. from CHCl3/petroleum ether; elem. anal.;
DOI:10.1016/0022-328X(92)83382-R