Morpholine, 4-(1-thioxobutyl)- (9CI)

Base Information

• Chemical Name: Morpholine, 4-(1-thioxobutyl)- (9CI)
• CAS No.: 5309-97-7
• Molecular Formula: C8H15 N O S
• Molecular Weight: 173.279
• Hs Code.: 2934999090
• Mol file: 5309-97-7.mol

Synonyms:Morpholine,4-(1-thioxobutyl)- (9CI); Morpholine, 4-(thiobutyryl)- (7CI,8CI); NSC 73058

Chemical Property of Morpholine, 4-(1-thioxobutyl)- (9CI)

Chemical Property:

• Vapor Pressure: 0.0194mmHg at 25°C
• Boiling Point: 252.4°C at 760 mmHg
• Flash Point: 106.4°C
• PSA: 44.56000
• Density: 1.078g/cm³
• LogP: 1.38400

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Morpholine, 4-(1-thioxobutyl)- (9CI)

There total 4 articles about Morpholine, 4-(1-thioxobutyl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

4-morpholinecarboxaldehyde (4394-85-8) + n-Butyl chloride (109-69-3) → 1--butanethione (5309-97-7)

Guidance literature:

With sulfur; sodium hydroxide; at 100 ℃; for 8h; Schlenk technique;

DOI:10.1002/ejoc.202100588

Reference yield: 70.0%

4-<1-(Diphenylphosphinoyl)butyl>morpholine (162274-55-7) → 1--butanethione (5309-97-7)

Guidance literature:

With sulfur; lithium diisopropyl amide; In tetrahydrofuran; at -20 ℃; for 0.333333h;

Reference yield: 56.0%

morpholine (110-91-8,99108-56-2) + butyraldehyde (123-72-8) → 1--butanethione (5309-97-7)

Guidance literature:

With sulfur; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

DOI:10.1055/s-1985-31114

upstream raw materials:

morpholine

butyraldehyde

butanone

4-<1-(Diphenylphosphinoyl)butyl>morpholine

Downstream raw materials:

ethylthioacetic acid methyl ester

ethylthioacetic acid ethyl ester

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