Technology Process of Oxazole, 2-(3,5-dimethyl-2-nitrophenyl)-
There total 5 articles about Oxazole, 2-(3,5-dimethyl-2-nitrophenyl)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: thionyl chloride; pyridine / 2 h / 50 °C
2: CH2Cl2 / 48 °C
3: thionyl chloride / CH2Cl2 / 1 h
4: 310 mg / NiO2 monohydrate / benzene / 48 h / Heating
5: H2SO4; KNO3 / 1 h
With
pyridine; nickel(IV) oxide; thionyl chloride; sulfuric acid; potassium nitrate;
In
dichloromethane; benzene;
DOI:10.1021/jm030528p
- Guidance literature:
-
Multi-step reaction with 4 steps
1: CH2Cl2 / 48 °C
2: thionyl chloride / CH2Cl2 / 1 h
3: 310 mg / NiO2 monohydrate / benzene / 48 h / Heating
4: H2SO4; KNO3 / 1 h
With
nickel(IV) oxide; thionyl chloride; sulfuric acid; potassium nitrate;
In
dichloromethane; benzene;
DOI:10.1021/jm030528p
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 310 mg / NiO2 monohydrate / benzene / 48 h / Heating
2: H2SO4; KNO3 / 1 h
With
nickel(IV) oxide; sulfuric acid; potassium nitrate;
In
benzene;
DOI:10.1021/jm030528p