4-(p-Tolylazo)-m-toluidine

Base Information

• Chemical Name: 4-(p-Tolylazo)-m-toluidine
• CAS No.: 3963-79-9
• Molecular Formula: C14H15N3
• Molecular Weight: 225.293
• Hs Code.: 2927000090
• DSSTox Substance ID: DTXSID001040451
• Nikkaji Number: J59.710D
• ChEMBL ID: CHEMBL84529
• Mol file: 3963-79-9.mol

Synonyms:4'-Amino-4-2'-azotoluene;4-(p-Tolylazo)-m-toluidine;BRN 0746646;3963-79-9;m-Toluidine, 4-(p-tolylazo)-;Benzenamine, 3-methyl-4-((4-methylphenyl)azo)-;4-16-00-00534 (Beilstein Handbook Reference);Benzenamine, 3-methyl-4-[(4-methylphenyl)azo]-;CHEMBL84529;SCHEMBL11434837;4,2'-Dimethylazobenzen-4'-amine;DTXSID001040451;LS-154414;Benzenamine, 3-methyl-4-((4-methylphenyl)azo)- (9CI);Benzenamine, 3-methyl-4-[2-(4-methylphenyl)diazenyl]-

Chemical Property of 4-(p-Tolylazo)-m-toluidine

Chemical Property:

• Vapor Pressure: 1.52E-06mmHg at 25°C
• Melting Point: 127°C
• Refractive Index: 1.5770 (estimate)
• Boiling Point: 398°Cat760mmHg
• Flash Point: 194.5°C
• PSA: 50.74000
• Density: 1.09g/cm³
• LogP: 4.88220
• XLogP3: 3.7
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 225.126597491
• Heavy Atom Count: 17
• Complexity: 256

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)N=NC2=C(C=C(C=C2)N)C

Technology Process of 4-(p-Tolylazo)-m-toluidine

There total 7 articles about 4-(p-Tolylazo)-m-toluidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

m-toluidine hydrochloride (638-03-9) + 1-amino-3-methylbenzene (108-44-1) + 1,3-di(p-tolyl)triaz-1-ene (785-86-4,813445-46-4) → 3-methyl-4-p-tolylazo-aniline (3963-79-9)

Guidance literature:

at 50 - 60 ℃;

Reference yield:

p-methylbenzenediazonium chloride (2028-84-4) + 1-amino-3-methylbenzene (108-44-1) → 3-methyl-4-p-tolylazo-aniline (3963-79-9)

Guidance literature:

With sodium acetate;

Reference yield:

p-methylbenzenediazonium chloride (2028-84-4) + m-toluidine hydrochloride (638-03-9) → N-m-tolyl-N'-p-tolyl-triazene (116531-08-9) + 3-methyl-4-p-tolylazo-aniline (3963-79-9)

Guidance literature:

With sodium acetate;

upstream raw materials:

p-methylbenzenediazonium chloride

m-toluidine hydrochloride

1-amino-3-methylbenzene

1,3-di(p-tolyl)triaz-1-ene

Downstream raw materials:

2-methyl-p-phenylenediamine

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