4-Ethenyl-1H-indole

Base Information

Chemical Name:4-Ethenyl-1H-indole
CAS No.:68900-05-0
Molecular Formula:C10H9N
Molecular Weight:143.188
Hs Code.:
Mol file:68900-05-0.mol

Synonyms:

Suppliers and Price of 4-Ethenyl-1H-indole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AccelPharmtech
4-ethenyl-1H-Indole 97.00%
25G
$ 7320.00

AccelPharmtech
4-ethenyl-1H-Indole 97.00%
5G
$ 3900.00

AccelPharmtech
4-ethenyl-1H-Indole 97.00%
1G
$ 2280.00

Total 3 raw suppliers

Chemical Property of 4-Ethenyl-1H-indole

Chemical Property:

PSA：15.79000
LogP:2.81090

Purity/Quality:

99% ^*data from raw suppliers

4-ethenyl-1H-Indole 97.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-Ethenyl-1H-indole

There total 10 articles about 4-Ethenyl-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1074-86-8
4-formyl indole

: 1779-49-3
Methyltriphenylphosphonium bromide

: 68900-05-0
4-vinylindole

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 2h; Inert atmosphere;

4-formyl indole; In tetrahydrofuran; hexane; at 20 ℃; for 8h; Inert atmosphere;
DOI:10.1021/jacs.0c08532

Reference yield: 34.0%

: 52488-36-5
4-bromo-1H-indole

: 75927-49-0
pinacol vinylboronate

: 68900-05-0
4-vinylindole

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; toluene; at 80 ℃; Inert atmosphere;
DOI:10.1002/anie.201801525

Reference yield:

: 59382-59-1
2-methyl-3-nitro-benzoic acid methyl ester

: 68900-05-0
4-vinylindole

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / dimethylformamide / 6 h / 130 °C

2: 82 percent / hydrogen / 10percent Pd/C / benzene / 1.5 h / 2585.7 Torr

3: 97 percent / diisobutylaluminium hydride / diethyl ether; toluene / -70 °C

4: 90.4 percent / active manganese dioxide / CH₂Cl₂ / 48 h / Ambient temperature

5: 1) n-BuLi / 1) THF, 30 min room temperature 2) THF, 1h below 30 deg C

With manganese(IV) oxide; n-butyllithium; hydrogen; diisobutylaluminium hydride; palladium on activated charcoal; In diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene; benzene;
DOI:10.1021/jo01304a043