Ethanone, 1-(5-methyl-2-nitrophenyl)-

Base Information

• Chemical Name: Ethanone, 1-(5-methyl-2-nitrophenyl)-
• CAS No.: 69976-70-1
• Molecular Formula: C9H9NO3
• Molecular Weight: 179.175
• Hs Code.: 2914700090
• Mol file: 69976-70-1.mol

Synonyms:1-(5-Methyl-2-nitro-phenyl)-aethanon;Ethanone,1-(5-methyl-2-nitrophenyl);5-methyl-2-nitroacetophenone;1(5-METHYL-2-NITROPHENYL) ETHANONE;

Chemical Property of Ethanone, 1-(5-methyl-2-nitrophenyl)-

Chemical Property:

• PSA: 62.89000
• LogP: 2.62900
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

1-(5-Methyl-2-nitrophenyl)ethan-1-one >97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethanone, 1-(5-methyl-2-nitrophenyl)-

There total 6 articles about Ethanone, 1-(5-methyl-2-nitrophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(5-methyl-2-nitro-benzoyl)-malonic acid diethyl ester (872270-50-3) → 1-(5-methyl-2-nitrophenyl)-ethanone (69976-70-1)

Guidance literature:

With sulfuric acid;

Reference yield:

5-methyl-2-nitrobenzoic acid (3113-72-2) → 1-(5-methyl-2-nitrophenyl)-ethanone (69976-70-1)

Guidance literature:

Multi-step reaction with 3 steps

1: phosphorus (V)-chloride

2: diethyl ether

3: aqueous sulfuric acid

With diethyl ether; phosphorus pentachloride; sulfuric acid;

Reference yield:

5-methyl-2-nitrobenzoyl chloride (38818-49-4) → 1-(5-methyl-2-nitrophenyl)-ethanone (69976-70-1)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

2: aqueous sulfuric acid

With diethyl ether; sulfuric acid;

upstream raw materials:

(5-methyl-2-nitro-benzoyl)-malonic acid diethyl ester

5-methyl-2-nitrobenzoyl chloride

diethyl malonate

5-methyl-2-nitrobenzoic acid

Downstream raw materials:

2-amino-5-methyl-acetophenone

1-(5-Bromomethyl-2-nitrophenyl)-ethanone

1-(5-(azidomethyl)-2-nitrophenyl)ethanol

1-(5-azidomethyl-2-nitrophenyl)ethanone

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