1-(cyclopenta-2,4-dien-1-ylidene)ethyl acetate

Base Information

Chemical Name:1-(cyclopenta-2,4-dien-1-ylidene)ethyl acetate
CAS No.:701-12-2
Molecular Formula:C9H10O2
Molecular Weight:168.19000
Hs Code.:2915390090
Mol file:701-12-2.mol

Synonyms:6-Acetoxy-6-methylfulven;Essigsaeure-(1-cyclopentadienyliden-aethylester);acetic acid-(1-cyclopentadienyliden-ethyl ester);6-acetoxy-6-methyl-fulvene;1-acetoxy-1-cyclopentadienylidene-ethane;6-(acetyloxy)-6-methylfulvene;Ethanol,1-(2,4-cyclopentadien-1-ylidene)-,acetate;

Suppliers and Price of 1-(cyclopenta-2,4-dien-1-ylidene)ethyl acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 1-(cyclopenta-2,4-dien-1-ylidene)ethyl acetate

Chemical Property:

PSA：57.53000
LogP:2.03530

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-(cyclopenta-2,4-dien-1-ylidene)ethyl acetate

There total 6 articles about 1-(cyclopenta-2,4-dien-1-ylidene)ethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: sodium cyclopentadienide

: 75-36-5
acetyl chloride

: 701-12-2
6-Acetoxy-6-methylfulven

Guidance literature:: In tetrahydrofuran; at 0 ℃;

Reference yield:

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 75-36-5
acetyl chloride

: 701-12-2
6-Acetoxy-6-methylfulven

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane; Yield given. Multistep reaction; 1.) a) THF, 0 deg C, b) -78 deg C, 10 min, 2.) from -78 deg C to RT, 10 min;
DOI:10.1021/jo00250a044