4-PHENYL-6-TRIFLUOROMETHYL-PYRIMIDINE-2-THIOL

Base Information

Chemical Name:4-PHENYL-6-TRIFLUOROMETHYL-PYRIMIDINE-2-THIOL
CAS No.:701920-69-6
Molecular Formula:C11H7F3N2S
Molecular Weight:256.24700
Hs Code.:
Mol file:701920-69-6.mol

Synonyms:6-Phenyl-4-trifluoromethyl-1H-pyrimidine-2-thione;4-trifluoromethyl-6-phenyl-pyrimidine-2-thione;4,6CF3PhpymSH;4,6-CF3PhpymSH;4,6-phenyltrifluoromethylpyrimidine-2-thione;

Suppliers and Price of 4-PHENYL-6-TRIFLUOROMETHYL-PYRIMIDINE-2-THIOL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
4-Phenyl-6-(trifluoromethyl)pyrimidine-2-thiol 97%
1g
$ 440.00

American Custom Chemicals Corporation
4-(TRIFLUOROMETHYL)-6-PHENYLPYRIMIDINE-2-THIOL 95.00%
1G
$ 1280.66

American Custom Chemicals Corporation
4-(TRIFLUOROMETHYL)-6-PHENYLPYRIMIDINE-2-THIOL 95.00%
250MG
$ 589.05

Total 3 raw suppliers

Chemical Property of 4-PHENYL-6-TRIFLUOROMETHYL-PYRIMIDINE-2-THIOL

Chemical Property:

PSA：60.77000
LogP:3.82500

Purity/Quality:

99% ^*data from raw suppliers

4-Phenyl-6-(trifluoromethyl)pyrimidine-2-thiol 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-PHENYL-6-TRIFLUOROMETHYL-PYRIMIDINE-2-THIOL

There total 2 articles about 4-PHENYL-6-TRIFLUOROMETHYL-PYRIMIDINE-2-THIOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 17356-08-0
thiourea

: 3108-32-5
1,1,1-trifluoro-4-phenylbut-3-en-2-one

: 701920-69-6
4-triluoromethylmethyl-6-phenylpyrimidine-2-thione

Guidance literature:: With sodium; In ethanol; for 24h; Heating;
DOI:10.1002/ejic.200400848

Reference yield:

: 100-52-7
benzaldehyde

: 701920-69-6
4-triluoromethylmethyl-6-phenylpyrimidine-2-thione

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / aq. NaOH / 18 h / 20 - 65 °C

2: 51 percent / sodium / ethanol / 24 h / Heating

With sodium hydroxide; sodium; In ethanol;
DOI:10.1002/ejic.200400848

Reference yield: 93.0%

: 701920-69-6
4-triluoromethylmethyl-6-phenylpyrimidine-2-thione

: 66-71-7
1,10-Phenanthroline

: 7440-02-0
nickel

: 1012051-11-4
[Ni(4,6-phenyltrifluoromethylpyrimidine-2-thione(-H))2(1,10-phenanthroline)]

Guidance literature:: With tetraethylammonium perchlorate; In acetonitrile; byproducts: H2; Electrolysis; acetonitrile soln. of ligands containing Et4NClO4 electrolysed using Pt wire as cathode and Ni as anode with direct current of 10 mA for 1.05 h at 5-37 V voltage; filtered; washed with acetonitrile and Et2O; dried at room temp.; elem. anal.;
DOI:10.1002/zaac.200600387