Benzenepropanoic acid, b-hydroxy-2-methoxy-, ethyl ester

Base Information

Chemical Name:Benzenepropanoic acid, b-hydroxy-2-methoxy-, ethyl ester
CAS No.:70200-18-9
Molecular Formula:C12H16O4
Molecular Weight:224.257
Hs Code.:

Synonyms:3-Hydroxy-3-(2-methoxy-phenyl)-propionic acid ethyl ester;ethyl 3-hydroxy-3-(2-methoxyphenyl)propanoate;Ethyl-3-hydroxy-3-(o-methoxyphenyl)-propionat;ethyl 3-hydroxy-3-(2-methoxyphenyl)propionate;(-)-ethyl 3-(2-methoxyphenyl)-3-hydroxypropionate;

Suppliers and Price of Benzenepropanoic acid, b-hydroxy-2-methoxy-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenepropanoic acid, b-hydroxy-2-methoxy-, ethyl ester

Chemical Property:

Boiling Point:127 °C (5 mmHg)
PSA：55.76000
Density:1.135±0.06 g/cm3(Predicted)
LogP:1.68180

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenepropanoic acid, b-hydroxy-2-methoxy-, ethyl ester

There total 10 articles about Benzenepropanoic acid, b-hydroxy-2-methoxy-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 4071-88-9
trimethylsilanyl-acetic acid ethyl ester

: 135-02-4
ortho-anisaldehyde

: 70200-18-9
ethyl 3-hydroxy-3-(2-methoxyphenyl)propionate

Guidance literature:: trimethylsilanyl-acetic acid ethyl ester; ortho-anisaldehyde; With 1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 24h; Inert atmosphere; Green chemistry;

With hydrogenchloride; In water; N,N-dimethyl-formamide; for 0.5h; Inert atmosphere; Green chemistry;
DOI:10.1016/j.tet.2012.11.015

Reference yield: 72.0%

: 41607-95-8
3-(2-methoxy-phenyl)-3-oxo-propionic acid ethyl ester

: 70200-18-9,138307-07-0,141545-24-6
(-)-3-hydroxy-3-(2-methoxyphenyl)propionic acid ethyl ester

Guidance literature:: 3-(2-methoxy-phenyl)-3-oxo-propionic acid ethyl ester; With diphenylsilane; (Ra)-BINAM-N-heterocyclic carbene-Rh(III); In tetrahydrofuran; at 15 ℃; for 72h;

With hydrogenchloride; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/jo062453d

Reference yield: 66.0%

: 105-36-2
ethyl bromoacetate

: 135-02-4
ortho-anisaldehyde

: 70200-18-9
ethyl 3-hydroxy-3-(2-methoxyphenyl)propionate

Guidance literature:: With boron trifluoride diethyl etherate; zinc; dibenzoyl peroxide; In tetrahydrofuran; water; at 20 ℃; for 9h;
DOI:10.1055/s-2000-6378