1-Hydroxy-2,8,9-trioxa-5-aza-1-germabicyclo(3.3.3)undecane

Base Information

• Chemical Name: 1-Hydroxy-2,8,9-trioxa-5-aza-1-germabicyclo(3.3.3)undecane
• CAS No.: 71682-43-4
• Molecular Formula: C6H13 Ge N O4
• Molecular Weight: 235.81
• Hs Code.: 2934999090
• Mol file: 71682-43-4.mol

Synonyms:1-Hydroxygermatrane;1-Germatranol;2,8,9-trioxa-5-aza-1-germabicyclo[3.3.3]undecan-1-ol;71682-43-4;BRN 4130418;1-Hydroxy-2,8,9-trioxa-5-aza-1-germabicyclo(3.3.3)undecane;2,8,9-Trioxa-5-aza-1-germabicyclo(3.3.3)undecane, 1-hydroxy-;SCHEMBL2349222;AKOS024456013

Chemical Property of 1-Hydroxy-2,8,9-trioxa-5-aza-1-germabicyclo(3.3.3)undecane

Chemical Property:

• Melting Point: 156-157 °C
• Boiling Point: 233.2±50.0 °C(Predicted)
• PKA: 4.83±0.20(Predicted)
• Flash Point: 185oC
• PSA: 40.16000
• LogP: -0.77610
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 0
• Exact Mass: 238.0134607
• Heavy Atom Count: 12
• Complexity: 113

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

1-HYDROXY-2,8,9-TRIOXA-5-AZA-1-GERMABICYCLO-(3.3.3)-UNDECANE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CO[Ge]2OCCN1CCO2.O

Technology Process of 1-Hydroxy-2,8,9-trioxa-5-aza-1-germabicyclo(3.3.3)undecane

There total 3 articles about 1-Hydroxy-2,8,9-trioxa-5-aza-1-germabicyclo(3.3.3)undecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triethanolamine (102-71-6,64114-46-1) + germanium dioxide → 1-germatranol (71682-43-4)

Guidance literature:

In water; at 90 ℃;

DOI:10.1016/j.jorganchem.2012.12.036

Reference yield:

1-hydroxygermatrane monohydrate (101182-23-4) → 1-germatranol (71682-43-4)

Guidance literature:

In neat (no solvent); byproducts: H2O; dehydration on heating to 50-60°C in vac.;

DOI:10.1007/BF00962326

Reference yield:

→ 1-germatranol (71682-43-4)

Guidance literature:

Germatran I, H2O;

upstream raw materials:

1-hydroxygermatrane monohydrate

triethanolamine

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