2-[[[(4-Chlorophenyl)amino]carbonyl]amino]-N,N,2-trimethylpropanamide

Base Information

Chemical Name:2-[[[(4-Chlorophenyl)amino]carbonyl]amino]-N,N,2-trimethylpropanamide
CAS No.:70974-11-7
Molecular Formula:C13H18ClN3O2
Molecular Weight:283.758
Hs Code.:
DSSTox Substance ID:DTXSID501155982

Synonyms:DTXSID501155982;2-[[[(4-Chlorophenyl)amino]carbonyl]amino]-N,N,2-trimethylpropanamide;70974-11-7

Suppliers and Price of 2-[[[(4-Chlorophenyl)amino]carbonyl]amino]-N,N,2-trimethylpropanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[[[(4-Chlorophenyl)amino]carbonyl]amino]-N,N,2-trimethylpropanamide

Chemical Property:

XLogP3:1.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:283.1087545
Heavy Atom Count:19
Complexity:337

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C(=O)N(C)C)NC(=O)NC1=CC=C(C=C1)Cl

Technology Process of 2-[[[(4-Chlorophenyl)amino]carbonyl]amino]-N,N,2-trimethylpropanamide

There total 5 articles about 2-[[[(4-Chlorophenyl)amino]carbonyl]amino]-N,N,2-trimethylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1613-88-3
4-chloro-N-hydroxybenzamide

: 54856-83-6
3-dimethylamino-2,2-dimethyl-2H-azirine

: 70974-11-7
1-(p-Chlorphenyl)-3-<1-dimethylcarbamoyl-1-methylethyl>-harnstoff

Guidance literature:: In tetrahydrofuran; for 96h;

Reference yield:

: 106-47-8
4-chloro-aniline

: 70974-11-7
1-(p-Chlorphenyl)-3-<1-dimethylcarbamoyl-1-methylethyl>-harnstoff

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / melt / 0.17 h / 140 °C

2: 92 percent / 1.) 1 n NaOH, 2.) 1 n HCl / 1.) 10 min, 45 deg C, 2.) 0 deg C

3: 1.) triethylamine, chloro ethylformate / 1.) THF, 15 min, -20 deg C, 30 min, 0 deg C, 2.) 1 h, -20 deg C, 2 h, 0 deg C

With hydrogenchloride; sodium hydroxide; chloro ethylformate; triethylamine; In melt;

Reference yield:

: 54213-21-7
α-Isocyanatobuttersaeure-methylester

: 70974-11-7
1-(p-Chlorphenyl)-3-<1-dimethylcarbamoyl-1-methylethyl>-harnstoff

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / melt / 0.17 h / 140 °C

2: 92 percent / 1.) 1 n NaOH, 2.) 1 n HCl / 1.) 10 min, 45 deg C, 2.) 0 deg C

3: 1.) triethylamine, chloro ethylformate / 1.) THF, 15 min, -20 deg C, 30 min, 0 deg C, 2.) 1 h, -20 deg C, 2 h, 0 deg C

With hydrogenchloride; sodium hydroxide; chloro ethylformate; triethylamine; In melt;