4-Hydroxy-1,6-bis(3-methoxyphenyl)hexan-3-one

Base Information

Chemical Name:4-Hydroxy-1,6-bis(3-methoxyphenyl)hexan-3-one
CAS No.:71505-81-2
Molecular Formula:C20H24O4
Molecular Weight:328.408
Hs Code.:
DSSTox Substance ID:DTXSID20501120

Synonyms:4-HYDROXY-1,6-BIS(3-METHOXYPHENYL)HEXAN-3-ONE;71505-81-2;DTXSID20501120

Suppliers and Price of 4-Hydroxy-1,6-bis(3-methoxyphenyl)hexan-3-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Hydroxy-1,6-bis(3-methoxyphenyl)hexan-3-one

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:9
Exact Mass:328.16745924
Heavy Atom Count:24
Complexity:371

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC(=C1)CCC(C(=O)CCC2=CC(=CC=C2)OC)O

Technology Process of 4-Hydroxy-1,6-bis(3-methoxyphenyl)hexan-3-one

There total 7 articles about 4-Hydroxy-1,6-bis(3-methoxyphenyl)hexan-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 40138-66-7
3-(m-methoxyphenyl)propanal

: 71505-81-2
4-Hydroxy-1,6-bis-(m-methoxyphenyl)-hexan-3-on

Guidance literature:: With Cl; triethylamine; In ethanol;
DOI:10.1016/S0960-894X(97)10099-3

Reference yield: 31.0%

: 50704-52-4
methyl 3-(3-methoxyphenyl)propionate

: 71505-81-2
4-Hydroxy-1,6-bis-(m-methoxyphenyl)-hexan-3-on

Guidance literature:: With sodium; In toluene; at 110 ℃;
DOI:10.1021/jo00030a039

Reference yield:

: 6099-04-3,17570-26-2
trans-3-methoxycinnamic acid

: 71505-81-2
4-Hydroxy-1,6-bis-(m-methoxyphenyl)-hexan-3-on

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Pd/C

2: LiAlH₄

3: PCC

4: 75 percent / 2)2C₃HNC(CH₃)Bn>Cl, Et₃N / ethanol

With lithium aluminium tetrahydride; Cl; hydrogen; triethylamine; pyridinium chlorochromate; palladium on activated charcoal; In ethanol;
DOI:10.1016/S0960-894X(97)10099-3