{[Chloro(dimethyl)silyl]methyl}(diphenyl)phosphane

Base Information

Chemical Name:{[Chloro(dimethyl)silyl]methyl}(diphenyl)phosphane
CAS No.:72447-46-2
Molecular Formula:C15H18ClPSi
Molecular Weight:292.82
Hs Code.:
DSSTox Substance ID:DTXSID70517736
Wikidata:Q82379906

Synonyms:72447-46-2;{[Chloro(dimethyl)silyl]methyl}(diphenyl)phosphane;SCHEMBL10384714;DTXSID70517736;((chlorodimethylsilyl)methyl)diphenylphosphane

Suppliers and Price of {[Chloro(dimethyl)silyl]methyl}(diphenyl)phosphane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of {[Chloro(dimethyl)silyl]methyl}(diphenyl)phosphane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:4
Exact Mass:292.0603918
Heavy Atom Count:18
Complexity:227

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(CP(C1=CC=CC=C1)C2=CC=CC=C2)Cl

Technology Process of {[Chloro(dimethyl)silyl]methyl}(diphenyl)phosphane

There total 3 articles about {[Chloro(dimethyl)silyl]methyl}(diphenyl)phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-78-5,30107-43-8
dimethylsilicon dichloride

: 1486-28-8
diphenyl(methyl)phosphine

: 72447-46-2
((chlorodimethylsilyl)methyl)diphenylphosphane

Guidance literature:: diphenyl(methyl)phosphine; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In hexane; at 0 - 20 ℃; for 60h; Inert atmosphere;

dimethylsilicon dichloride; In hexane; at -35 - 20 ℃; Inert atmosphere;
DOI:10.1007/s11243-018-0276-7

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 72447-46-2
((chlorodimethylsilyl)methyl)diphenylphosphane

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethyl ether / -35 °C / Inert atmosphere

2.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / hexane / 60 h / 0 - 20 °C / Inert atmosphere

2.2: -35 - 20 °C / Inert atmosphere

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In diethyl ether; hexane;
DOI:10.1007/s11243-018-0276-7