[(Dimethylsilyl)methyl](diphenyl)phosphane

Base Information

Chemical Name:[(Dimethylsilyl)methyl](diphenyl)phosphane
CAS No.:86934-50-1
Molecular Formula:C15H19PSi
Molecular Weight:258.375
Hs Code.:
DSSTox Substance ID:DTXSID00833158

Synonyms:[(Dimethylsilyl)methyl](diphenyl)phosphane;SCHEMBL10384229;DTXSID00833158;86934-50-1

Suppliers and Price of [(Dimethylsilyl)methyl](diphenyl)phosphane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [(Dimethylsilyl)methyl](diphenyl)phosphane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:4
Exact Mass:257.09153911
Heavy Atom Count:17
Complexity:187

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)CP(C1=CC=CC=C1)C2=CC=CC=C2

Technology Process of [(Dimethylsilyl)methyl](diphenyl)phosphane

There total 3 articles about [(Dimethylsilyl)methyl](diphenyl)phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 3144-74-9
chloromethyldimethylsilane

: 829-85-6
diphenylphosphane

: 86934-50-1
((dimethylsilyl)methyl)diphenylphosphane

Guidance literature:: diphenylphosphane; With n-butyllithium; In tetrahydrofuran; hexane; at -80 - 20 ℃; for 3.5h; Inert atmosphere; Schlenk technique;

chloromethyldimethylsilane; In tetrahydrofuran; hexane; at -40 - 20 ℃; Schlenk technique; Inert atmosphere;
DOI:10.1021/ic502968z

Reference yield: 80.0%

: 72447-46-2
((chlorodimethylsilyl)methyl)diphenylphosphane

: 86934-50-1
((dimethylsilyl)methyl)diphenylphosphane

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 20 ℃; for 1h;

Reference yield:

: ((diphenylphosphino)methyl)lithium N,N,N',N'-tetramethyl-1,2-diaminoethane

: 86934-50-1
((dimethylsilyl)methyl)diphenylphosphane

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / tetrahydrofuran / 2 h / -78 °C

2: 80 percent / LiAlH₄ / diethyl ether / 1 h / 20 °C

With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether;