Hexanedioic acid, bis[2-[[(phenylmethyl)amino]thioxomethyl]hydrazide]

Base Information

• Chemical Name: Hexanedioic acid, bis[2-[[(phenylmethyl)amino]thioxomethyl]hydrazide]
• CAS No.: 72743-58-9
• Molecular Formula: C22H28N6O2S2
• Molecular Weight: 472.635
• Mol file: 72743-58-9.mol

Synonyms:

Chemical Property of Hexanedioic acid, bis[2-[[(phenylmethyl)amino]thioxomethyl]hydrazide]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Hexanedioic acid, bis[2-[[(phenylmethyl)amino]thioxomethyl]hydrazide]

There total 1 articles about Hexanedioic acid, bis[2-[[(phenylmethyl)amino]thioxomethyl]hydrazide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.7%

Benzyl isothiocyanate (622-78-6) + adipic acid dihydrazide (1071-93-8,98152-55-7) → 4,4'-dibenzyl bis adipyl thiosemicarbazide (72743-58-9)

Guidance literature:

In methanol; for 4h; Heating;

Reference yield: 93.7%

4,4'-dibenzyl bis adipyl thiosemicarbazide (72743-58-9) → C22H24N6S2

Guidance literature:

With sulfuric acid; for 2h; Ambient temperature;

Reference yield: 80.0%

4,4'-dibenzyl bis adipyl thiosemicarbazide (72743-58-9) → C22H24N6S2

Guidance literature:

With sodium hydroxide; In water; for 4h; Heating;

upstream raw materials:

Benzyl isothiocyanate

adipic acid dihydrazide

Refernces