{5-[1-(3-amino-4-chlorophenyl)-2,2-dichlorovinyl]-2-chlorophenyl}amine

Base Information

• Chemical Name: {5-[1-(3-amino-4-chlorophenyl)-2,2-dichlorovinyl]-2-chlorophenyl}amine
• CAS No.: 73046-20-5
• Molecular Formula: C14H10Cl4N2
• Molecular Weight: 348.05500
• Hs Code.: 2921590090
• Mol file: 73046-20-5.mol

Synonyms:1,1-Dichlor-2,2-bis-(4-chlor-3-aminophenyl)-ethylen;Benzene,1,1'-(2,2-dibromo-3-methylcyclopropylidene)bis;1,1-Bis-(3-amino-4-chlor-phenyl)-2,2-dichlor-aethen;1,1-dibromo-2,2-diphenyl-3-methylcyclopropane;1,1-bis-(3-amino-4-chloro-phenyl)-2,2-dichloro-ethene;2.2-Dichlor-1.1-bis-(4-chlor-3-amino-phenyl)-aethylen;2.2-Dibromo-1.1-diphenyl-3-methylcyclopropan;

Chemical Property of {5-[1-(3-amino-4-chlorophenyl)-2,2-dichlorovinyl]-2-chlorophenyl}amine

Chemical Property:

• Melting Point: 143-144 °C
• Boiling Point: 487.3±45.0 °C(Predicted)
• PKA: 2.13±0.10(Predicted)
• PSA: 52.04000
• Density: 1.504±0.06 g/cm3(Predicted)
• LogP: 6.51470

Purity/Quality:

98%min ^*data from raw suppliers

{5-[1-(3-Amino-4-chlorophenyl)-2,2-dichlorovinyl]-2-chlorophenyl}amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of {5-[1-(3-amino-4-chlorophenyl)-2,2-dichlorovinyl]-2-chlorophenyl}amine

There total 4 articles about {5-[1-(3-amino-4-chlorophenyl)-2,2-dichlorovinyl]-2-chlorophenyl}amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1-dichloro-2,2-bis(4-chloro-3-nitrophenyl)ethylene (73046-19-2) → 1,1-bis-(3-amino-4-chloro-phenyl)-2,2-dichloro-ethene (73046-20-5)

Guidance literature:

With sodium dithionite; acetic acid;

DOI:10.1039/jr9450000803

Reference yield:

1,1,1-trichloro-2,2-bis(3-nitro-4-chlorophenyl)ethane (4399-07-9) → 1,1-bis-(3-amino-4-chloro-phenyl)-2,2-dichloro-ethene (73046-20-5)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanolic KOH

2: sodium dithionite; aqueous acetic acid

With potassium hydroxide; sodium dithionite; acetic acid;

DOI:10.1039/jr9450000803

Reference yield:

p,p'-DDT (50-29-3,29411-63-0) → 1,1-bis-(3-amino-4-chloro-phenyl)-2,2-dichloro-ethene (73046-20-5)

Guidance literature:

Multi-step reaction with 3 steps

1: HNO₃ / acetic acid

2: Py / Heating

3: Na₂S₂O₄ / acetic acid

With pyridine; sodium dithionite; nitric acid; In acetic acid;

upstream raw materials:

1,1-dichloro-2,2-bis(4-chloro-3-nitrophenyl)ethylene

acetic acid

1,1,1-trichloro-2,2-bis(3-nitro-4-chlorophenyl)ethane

p,p'-DDT

Downstream raw materials:

1,1-dichloro-2,2-bis(4-chloro-3-isocyanatophenyl)ethylene

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