1,3-Diphenyl-5-dodecylbarbituric acid

Base Information

• Chemical Name: 1,3-Diphenyl-5-dodecylbarbituric acid
• CAS No.: 73481-00-2
• Molecular Formula: C₁₂H₁₃NO
• Molecular Weight: 187.241
• Mol file: 73481-00-2.mol

Synonyms:8-Methoxy-1,3-dimethyl-isoquinoline;

Chemical Property of 1,3-Diphenyl-5-dodecylbarbituric acid

Chemical Property:

• PSA: 22.12000
• LogP: 2.86020

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-Diphenyl-5-dodecylbarbituric acid

There total 4 articles about 1,3-Diphenyl-5-dodecylbarbituric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

1-(2-Acetyl-3-methoxyphenyl)-2-propanon (82958-27-8) → 1-Amino-8-methoxy-3-methylnaphthalin (82958-24-5) + 8-Methoxy-1,3-dimethylisochinolin (73481-00-2)

Guidance literature:

With ammonia; In methanol; at 25 ℃;

DOI:10.1016/S0040-4039(00)87246-9

Reference yield: 84.0%

8-Hydroxy-1,3-dimethylisochinolinium-chlorid (65690-45-1) + dimethyl sulfate (77-78-1) → 8-Methoxy-1,3-dimethylisochinolin (73481-00-2)

Guidance literature:

With benzyltri(n-butyl)ammonium chloride;

Reference yield: 83.0%

1-<2-Acetyl-3-hydroxy-5-(2-hydroxyethoxy)phenyl>-2-propanon (81782-32-3) → 1-Amino-8-methoxy-3-methylnaphthalin (82958-24-5) + 8-Methoxy-1,3-dimethylisochinolin (73481-00-2)

Guidance literature:

With hydrogenchloride; ammonium hydroxide; In methanol; 1) 12 h, 2) 24 h;

upstream raw materials:

1-(2-Acetyl-3-methoxyphenyl)-2-propanon

1-<2-Acetyl-3-hydroxy-5-(2-hydroxyethoxy)phenyl>-2-propanon

8-Hydroxy-1,3-dimethylisochinolinium-chlorid

dimethyl sulfate

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