[(Methylphosphanediyl)di(propane-3,1-diyl)]bis(diphenylphosphane)

Base Information

Chemical Name:[(Methylphosphanediyl)di(propane-3,1-diyl)]bis(diphenylphosphane)
CAS No.:73731-95-0
Molecular Formula:C31H35P3
Molecular Weight:500.54
Hs Code.:
DSSTox Substance ID:DTXSID00502332
Wikidata:Q82355256

Synonyms:73731-95-0;DTXSID00502332;[(Methylphosphanediyl)di(propane-3,1-diyl)]bis(diphenylphosphane)

Suppliers and Price of [(Methylphosphanediyl)di(propane-3,1-diyl)]bis(diphenylphosphane)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of [(Methylphosphanediyl)di(propane-3,1-diyl)]bis(diphenylphosphane)

Chemical Property:

Boiling Point:603.0±40.0 °C(Predicted)
PSA：40.77000
LogP:7.14410
XLogP3:6.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:12
Exact Mass:500.19516211
Heavy Atom Count:34
Complexity:431

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CP(CCCP(C1=CC=CC=C1)C2=CC=CC=C2)CCCP(C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of [(Methylphosphanediyl)di(propane-3,1-diyl)]bis(diphenylphosphane)

There total 4 articles about [(Methylphosphanediyl)di(propane-3,1-diyl)]bis(diphenylphosphane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 593-54-4
methylphosphine

: 57137-55-0
3-(diphenylphosphino)propyl chloride

: 73727-00-1
Diphenyl<3-(methylphosphino)propyl>phosphin

: 73731-95-0
Bis<3-(diphenylphosphino)propyl>methylphosphin

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given; 1.) DME, hexane, -60 - -65 deg C; 2.) DME, RT, overnight;

Reference yield:

: 829-85-6
diphenylphosphane

: 73731-95-0
Bis<3-(diphenylphosphino)propyl>methylphosphin

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi / 1.) hexane, THF, RT, 1 h; 2.) toluene, -78 deg C to RT, overnight

2: 1.) n-BuLi / 1.) hexane, DME, -60 deg C; 2.) DME, 2 h

3: 1.) n-BuLi / 1.) hexane, DME, RT, 30 min; 2.) DME

With n-butyllithium;

Reference yield:

: 57137-55-0
3-(diphenylphosphino)propyl chloride

: 73731-95-0
Bis<3-(diphenylphosphino)propyl>methylphosphin

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) hexane, DME, -60 deg C; 2.) DME, 2 h

2: 1.) n-BuLi / 1.) hexane, DME, RT, 30 min; 2.) DME

With n-butyllithium;