Dimethyl (4-bromophenyl)arsonite

Base Information

• Chemical Name: Dimethyl (4-bromophenyl)arsonite
• CAS No.: 73777-26-1
• Molecular Formula: C₈H₁₀AsBrO₂
• Molecular Weight: 292.992
• DSSTox Substance ID: DTXSID70542922
• Wikidata: Q82419724

Synonyms:73777-26-1;Dimethyl (4-bromophenyl)arsonite;dimethyl p-bromophenylarsonite;DTXSID70542922

Chemical Property of Dimethyl (4-bromophenyl)arsonite

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 291.90801
• Heavy Atom Count: 12
• Complexity: 122

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CO[As](C1=CC=C(C=C1)Br)OC

Technology Process of Dimethyl (4-bromophenyl)arsonite

There total 1 articles about Dimethyl (4-bromophenyl)arsonite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.5%

p-bromophenylarsine dichloride (73013-32-8) + sodium methylate (124-41-4) → dimethyl ester of p-bromophenyl-arsonous acid (73777-26-1)

Guidance literature:

In methanol; benzene; Ambient temperature;

Reference yield: 90.0%

phthalyl alcohol (612-14-6) + dimethyl ester of p-bromophenyl-arsonous acid (73777-26-1) → 2-(p-bromophenyl)-5,6-benzo-1,3,2-dioxarsepin (88861-61-4)

Guidance literature:

DOI:10.1007/BF00959193

Reference yield: 83.7%

1,2-bis(mercaptomethyl)benzene (41383-84-0) + dimethyl ester of p-bromophenyl-arsonous acid (73777-26-1) → 3-(p-bromophenyl)-4H,7H-5,6-benz-1,3,2-dithiaarsepine (118542-61-3)

Guidance literature:

In tetrachloromethane; for 2h; Heating;

DOI:10.1007/BF00962681

upstream raw materials:

p-bromophenylarsine dichloride

sodium methylate

Downstream raw materials:

C₂₄H₄₆AsBrO₆S₂Si₂

3-(p-bromophenyl)-4H,7H-5,6-benz-1,3,2-dithiaarsepine

2-(p-bromophenyl)-5,6-benzo-1,3,2-dioxarsepin

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