1,2,4-Nonanetriol, 4-acetate 1-(4-methylbenzenesulfonate), (2R,4R)-

Base Information

Chemical Name:1,2,4-Nonanetriol, 4-acetate 1-(4-methylbenzenesulfonate), (2R,4R)-
CAS No.:741679-96-9
Molecular Formula:C₁₈H₂₈O₆S
Molecular Weight:372.483
Hs Code.:

Synonyms:

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Chemical Property of 1,2,4-Nonanetriol, 4-acetate 1-(4-methylbenzenesulfonate), (2R,4R)-

Chemical Property:

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Technology Process of 1,2,4-Nonanetriol, 4-acetate 1-(4-methylbenzenesulfonate), (2R,4R)-

There total 3 articles about 1,2,4-Nonanetriol, 4-acetate 1-(4-methylbenzenesulfonate), (2R,4R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35192-73-5
non-1-en-4-ol

: 741679-96-9
Acetic acid (R)-1-[(R)-2-hydroxy-3-(toluene-4-sulfonyloxy)-propyl]-hexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 47 percent / Amano lipase from Pseudomonas fluorescens / hexane / 26 h / 20 °C

2: 88 percent / K₃Fe(CN)6; OsO₄; (DHQD)2PHAL / K₂CO₃ / 2-methyl-propan-2-ol; H₂O / 24 h / 0 °C

3: 75 percent / pyridine / CH₂Cl₂ / 27 h / 20 °C

With pyridine; osmium(VIII) oxide; Amano lipase from Pseudomonas fluorescens; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III); potassium carbonate; In hexane; dichloromethane; water; tert-butyl alcohol; 2: Sharpless asymmetric dihydroxylation;
DOI:10.1016/j.tetlet.2004.05.149

Reference yield:

: 66-25-1
hexanal

: 741679-96-9
Acetic acid (R)-1-[(R)-2-hydroxy-3-(toluene-4-sulfonyloxy)-propyl]-hexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / Zn; aq.NH₄Cl / tetrahydrofuran / 1 h / 20 °C

2: 47 percent / Amano lipase from Pseudomonas fluorescens / hexane / 26 h / 20 °C

3: 88 percent / K₃Fe(CN)6; OsO₄; (DHQD)2PHAL / K₂CO₃ / 2-methyl-propan-2-ol; H₂O / 24 h / 0 °C

4: 75 percent / pyridine / CH₂Cl₂ / 27 h / 20 °C

With pyridine; osmium(VIII) oxide; Amano lipase from Pseudomonas fluorescens; ammonium chloride; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III); zinc; potassium carbonate; In tetrahydrofuran; hexane; dichloromethane; water; tert-butyl alcohol; 1: Barbier-Grignard reaction / 3: Sharpless asymmetric dihydroxylation;
DOI:10.1016/j.tetlet.2004.05.149

Reference yield:

: 741679-94-7
(R)-non-1-en-4-yl acetate

: 741679-96-9
Acetic acid (R)-1-[(R)-2-hydroxy-3-(toluene-4-sulfonyloxy)-propyl]-hexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / K₃Fe(CN)6; OsO₄; (DHQD)2PHAL / K₂CO₃ / 2-methyl-propan-2-ol; H₂O / 24 h / 0 °C

2: 75 percent / pyridine / CH₂Cl₂ / 27 h / 20 °C

With pyridine; osmium(VIII) oxide; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III); potassium carbonate; In dichloromethane; water; tert-butyl alcohol; 1: Sharpless asymmetric dihydroxylation;
DOI:10.1016/j.tetlet.2004.05.149