1,3-Dibenzyl-2-chloro-1,3,2-diazaphospholidine

Base Information

Chemical Name:1,3-Dibenzyl-2-chloro-1,3,2-diazaphospholidine
CAS No.:74731-09-2
Molecular Formula:C16H18ClN2P
Molecular Weight:304.759
Hs Code.:
DSSTox Substance ID:DTXSID60502772
Wikidata:Q82356074

Synonyms:1,3-Dibenzyl-2-chloro-1,3,2-diazaphospholidine;74731-09-2;DTXSID60502772

Suppliers and Price of 1,3-Dibenzyl-2-chloro-1,3,2-diazaphospholidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-Dibenzyl-2-chloro-1,3,2-diazaphospholidine

Chemical Property:

XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:304.0896133
Heavy Atom Count:20
Complexity:262

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CN(P(N1CC2=CC=CC=C2)Cl)CC3=CC=CC=C3

Technology Process of 1,3-Dibenzyl-2-chloro-1,3,2-diazaphospholidine

There total 1 articles about 1,3-Dibenzyl-2-chloro-1,3,2-diazaphospholidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 140-28-3,87170-83-0
N,N'-Dibenzylethylenediamine

: 74731-09-2
2-chloro-1,3-dibenzyl-1,3,2-diazaphospholidine

Guidance literature:: With triethylamine; phosphorus trichloride; In dichloromethane; at 0 ℃; for 1h; Schlenk technique;
DOI:10.1021/acs.chemmater.0c01561

Reference yield: 86.0%

: 109-89-7
diethylamine

: 74731-09-2
2-chloro-1,3-dibenzyl-1,3,2-diazaphospholidine

: 70819-41-9
N,N-diethyl-1,3-dibenzyl-1,3,2-diazaphospholidin-2-amine

Guidance literature:: With triethylamine; In diethyl ether; for 0.333333h;
DOI:10.1021/acs.chemmater.0c01561

Reference yield: 72.0%

: 12107-35-6
Na[CpMo(CO)3]

: 74731-09-2
2-chloro-1,3-dibenzyl-1,3,2-diazaphospholidine

: (C₅H₅)Mo(CO)2P(N(CH₂C₆H₅)CH₂CH₂N(CH₂C₆H₅))

Guidance literature:: In tetrahydrofuran; byproducts: carbon monoxide, NaCl; aminophosphine was added to a soln. of Mo-complex in THF at -78°C under inert atmosphere, soln. was stirred and slowly warmed to 25°C, mixt. was stirred for 12 h at 25°C; filtered under dry N2, filtrate was evapd., extd. into benzene, filtered, filtrate evapd. to dryness, residue was washed with cold hexane; elem. anal.;
DOI:10.1016/0022-328X(87)87111-5