2-Propenoic acid, 3-phenyl-, 2-acetylphenyl ester

Base Information

• Chemical Name: 2-Propenoic acid, 3-phenyl-, 2-acetylphenyl ester
• CAS No.: 74766-95-3
• Molecular Formula: C17H14O3
• Molecular Weight: 266.296
• Mol file: 74766-95-3.mol

Synonyms:

Chemical Property of 2-Propenoic acid, 3-phenyl-, 2-acetylphenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Propenoic acid, 3-phenyl-, 2-acetylphenyl ester

There total 10 articles about 2-Propenoic acid, 3-phenyl-, 2-acetylphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

o-hydroxyacetophenone (118-93-4,104809-67-8) + Cinnamoyl chloride (102-92-1,17082-09-6) → 2-acetylphenyl (E)-3-phenylacrylate (74766-95-3)

Guidance literature:

With pyridine; for 2h; Ambient temperature;

DOI:10.1002/jhet.5570350140

Reference yield:

o-hydroxyacetophenone (118-93-4,104809-67-8) + Cinnamic acid (621-82-9) → Zimtsaeure-<2-acetyl-phenyl >-ester (74766-95-3)

Guidance literature:

With pyridine; trichlorophosphate; at 20 ℃; Cooling with ice;

DOI:10.3390/molecules191016058

Reference yield:

(E)-2-(2-(methylthio)vinyl)-4H-chromen-4-one + o-hydroxyacetophenone (118-93-4,104809-67-8) → 2-acetylphenyl (E)-3-phenylacrylate (74766-95-3)

Guidance literature:

(E)-2-(2-(methylthio)vinyl)-4H-chromen-4-one; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; Inert atmosphere;

o-hydroxyacetophenone; With potassium hydroxide; for 0.166667h; Sonication;

DOI:10.1021/acs.orglett.8b03148

upstream raw materials:

cinnamoyl chloride

o-hydroxyacetophenone

Cinnamic acid

benzaldehyde

Downstream raw materials:

1-(2-hydroxyphenyl)-5-phenyl-4-pentene-1,3-dione

(E)-2-styrylchromone

2-cinnamoyl-3(2H)-benzofuranone

3-bromo-2-styrylchromone